C₃₇H₅₇NO₇Si

Base Information

Chemical Name:C₃₇H₅₇NO₇Si
CAS No.:1148112-28-0
Molecular Formula:C₃₇H₅₇NO₇Si
Molecular Weight:655.948
Hs Code.:

C<sub>37</sub>H<sub>57</sub>NO<sub>7</sub>Si

Synonyms:C₃₇H₅₇NO₇Si

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Chemical Property of C₃₇H₅₇NO₇Si

Chemical Property:

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Technology Process of C₃₇H₅₇NO₇Si

There total 8 articles about C₃₇H₅₇NO₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: C₂₇H₄₀O₃Si

: 138603-63-1
1-(2-pyrimidinethio) 3,4,6-trideoxy-2-O-methoxycarbonyl-3-(dimethylamino)-D-xylo-hexopyranoside

: 1148112-28-0
C₃₇H₅₇NO₇Si

Guidance literature:: With silver trifluoromethanesulfonate; In dichloromethane; toluene; at 0 - 2 ℃; for 4h; chemoselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1002/anie.200805334

Reference yield:

: 72297-78-0
(2S)-(tert-butyl)(3-iodo-2-methylpropoxy)diphenylsilane

: 1148112-28-0
C₃₇H₅₇NO₇Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: sec.-butyllithium / tetrahydrofuran; cyclohexane / 2 h / -98 °C

1.2: 0 - 1 °C

2.1: triethylamine; (S)-Ph,(R)-tBu-CuCl₂(C₅H₃NBrCHNCH(tBu)C₃H₃NO(Ph)) / tetrahydrofuran / 0.5 h / 20 °C

3.1: triethylamine; methanesulfonyl chloride / 0.5 h / -78 °C

3.2: 6 h / 20 °C

4.1: methanol; potassium carbonate / 2 h / 20 °C

5.1: triethylamine; sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 1 h / 0 °C

6.1: tetrahydrofuran / 16 h / -78 °C

7.1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran; toluene / 8 h / 0 °C

8.1: silver trifluoromethanesulfonate / dichloromethane; toluene / 4 h / 0 - 20 °C / Molecular sieve

With methanol; (S)-Ph,(R)-tBu-CuCl₂(C₅H₃NBrCHNCH(tBu)C₃H₃NO(Ph)); sec.-butyllithium; silver trifluoromethanesulfonate; sulfur trioxide pyridine complex; potassium carbonate; methanesulfonyl chloride; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; dichloromethane; cyclohexane; dimethyl sulfoxide; toluene;

Reference yield:

: 1148112-25-7
C₂₃H₃₄O₄Si

: 1148112-28-0
C₃₇H₅₇NO₇Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: triethylamine; (S)-Ph,(R)-tBu-CuCl₂(C₅H₃NBrCHNCH(tBu)C₃H₃NO(Ph)) / tetrahydrofuran / 0.5 h / 20 °C

2.1: triethylamine; methanesulfonyl chloride / 0.5 h / -78 °C

2.2: 6 h / 20 °C

3.1: methanol; potassium carbonate / 2 h / 20 °C

4.1: triethylamine; sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 1 h / 0 °C

5.1: tetrahydrofuran / 16 h / -78 °C

6.1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran; toluene / 8 h / 0 °C

7.1: silver trifluoromethanesulfonate / dichloromethane; toluene / 4 h / 0 - 20 °C / Molecular sieve

With methanol; (S)-Ph,(R)-tBu-CuCl₂(C₅H₃NBrCHNCH(tBu)C₃H₃NO(Ph)); silver trifluoromethanesulfonate; sulfur trioxide pyridine complex; potassium carbonate; methanesulfonyl chloride; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; toluene;