2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-1-octyl 4-(bromomethyl)-3-nitrobenzoate

Base Information

Chemical Name:2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-1-octyl 4-(bromomethyl)-3-nitrobenzoate
CAS No.:448960-13-2
Molecular Formula:C₁₆H₇BrF₁₅NO₄
Molecular Weight:642.116
Hs Code.:

Synonyms:2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-1-octyl 4-(bromomethyl)-3-nitrobenzoate

Suppliers and Price of 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-1-octyl 4-(bromomethyl)-3-nitrobenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-1-octyl 4-(bromomethyl)-3-nitrobenzoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-1-octyl 4-(bromomethyl)-3-nitrobenzoate

There total 1 articles about 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-1-octyl 4-(bromomethyl)-3-nitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 307-30-2
2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-1-octanol

: 55715-03-2
4-bromomethyl-3-nitrobenzoic acid

: 448960-13-2
2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-1-octyl 4-(bromomethyl)-3-nitrobenzoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃;
DOI:10.1021/ja025835j

Reference yield: 32.0%

: 112-38-9
10-undecenoic acid

: 448960-13-2
2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-1-octyl 4-(bromomethyl)-3-nitrobenzoate

: 448960-14-3
2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-1-octyl 4-(1-oxo-10-undecenyloxymethyl)-3-nitrobenzoate

Guidance literature:: 10-undecenoic acid; With sodium hydroxide; In N,N,N,N,N,N-hexamethylphosphoric triamide; water; at 20 ℃; for 2h;

2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-1-octyl 4-(bromomethyl)-3-nitrobenzoate; In N,N,N,N,N,N-hexamethylphosphoric triamide; water; Further stages.;
DOI:10.1021/ja025835j

Reference yield:

: 448960-13-2
2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-1-octyl 4-(bromomethyl)-3-nitrobenzoate

: 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-1-octyl 4-(11-trichlorosilyl-1-oxoundecyl oxymethyl)-3-nitrobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: aq. NaOH / hexamethylphosphoric acid triamide / 2 h / 20 °C

1.2: 32 percent / hexamethylphosphoric acid triamide / 20 °C

2.1: trichlorosilane; hydrogen hexachloroplatinate(IV) hydrate / propan-2-ol / Heating

With dihydrogen hexachloroplatinate; sodium hydroxide; trichlorosilane; In N,N,N,N,N,N-hexamethylphosphoric triamide; isopropyl alcohol;
DOI:10.1021/ac020269w