Methyl-carbamic acid 5-methylcarbamoyloxymethyl-3-phenyl-3H-imidazol-4-ylmethyl ester

Base Information

Chemical Name:Methyl-carbamic acid 5-methylcarbamoyloxymethyl-3-phenyl-3H-imidazol-4-ylmethyl ester
CAS No.:117120-84-0
Molecular Formula:C₁₅H₁₈N₄O₄
Molecular Weight:318.332
Hs Code.:

Synonyms:Methyl-carbamic acid 5-methylcarbamoyloxymethyl-3-phenyl-3H-imidazol-4-ylmethyl ester

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Chemical Property of Methyl-carbamic acid 5-methylcarbamoyloxymethyl-3-phenyl-3H-imidazol-4-ylmethyl ester

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Technology Process of Methyl-carbamic acid 5-methylcarbamoyloxymethyl-3-phenyl-3H-imidazol-4-ylmethyl ester

There total 3 articles about Methyl-carbamic acid 5-methylcarbamoyloxymethyl-3-phenyl-3H-imidazol-4-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 624-83-9
methyl isocyanate

: 33457-06-6
(1-phenyl-1H-imidazole-4,5-diyl)-bis-methanol

: 117120-84-0
Methyl-carbamic acid 5-methylcarbamoyloxymethyl-3-phenyl-3H-imidazol-4-ylmethyl ester

Guidance literature:: With pyridine; In dichloromethane; for 24h; Ambient temperature;
DOI:10.1021/jm00121a023

Reference yield:

: 117121-01-4
diethyl 1-phenyl-1H-imidazole-4,5-dicarboxylate

: 117120-84-0
Methyl-carbamic acid 5-methylcarbamoyloxymethyl-3-phenyl-3H-imidazol-4-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / LiAlH₄ / CH₂Cl₂; diethyl ether / a) 0 - 5 deg C, 3 h, b) room temperature, 1 h

2: 38 percent / pyridine / CH₂Cl₂ / 24 h / Ambient temperature

With pyridine; lithium aluminium tetrahydride; In diethyl ether; dichloromethane;
DOI:10.1021/jm00121a023

Reference yield:

: 117121-07-0
diethyl 2-mercapto-1-phenylimidazole-4,5-dicarboxylate

: 117120-84-0
Methyl-carbamic acid 5-methylcarbamoyloxymethyl-3-phenyl-3H-imidazol-4-ylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / conc. nitric acid, sodium nitrite / H₂O / 1 h / 33 - 38 °C

2: 65 percent / LiAlH₄ / CH₂Cl₂; diethyl ether / a) 0 - 5 deg C, 3 h, b) room temperature, 1 h

3: 38 percent / pyridine / CH₂Cl₂ / 24 h / Ambient temperature

With pyridine; lithium aluminium tetrahydride; nitric acid; sodium nitrite; In diethyl ether; dichloromethane; water;
DOI:10.1021/jm00121a023