1,1-dimethylethyl 4-[2-(benzyloxycarbonyl)phenyl]-3,5-dibenzyloxybenzoate

Base Information

Chemical Name:1,1-dimethylethyl 4-[2-(benzyloxycarbonyl)phenyl]-3,5-dibenzyloxybenzoate
CAS No.:197804-84-5
Molecular Formula:C₃₉H₃₆O₆
Molecular Weight:600.711
Hs Code.:

Synonyms:1,1-dimethylethyl 4-[2-(benzyloxycarbonyl)phenyl]-3,5-dibenzyloxybenzoate

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Chemical Property of 1,1-dimethylethyl 4-[2-(benzyloxycarbonyl)phenyl]-3,5-dibenzyloxybenzoate

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Technology Process of 1,1-dimethylethyl 4-[2-(benzyloxycarbonyl)phenyl]-3,5-dibenzyloxybenzoate

There total 3 articles about 1,1-dimethylethyl 4-[2-(benzyloxycarbonyl)phenyl]-3,5-dibenzyloxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 67460-09-7
benzyl 2-bromobenzoate

: 197804-80-1
2,6-dibenzyloxy-4-(1,1-dimethylethoxycarbonyl)phenylboronic acid

: 197804-84-5
1,1-dimethylethyl 4-[2-(benzyloxycarbonyl)phenyl]-3,5-dibenzyloxybenzoate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In 1,4-dioxane; for 60h; Heating;
DOI:10.1021/jm020018f

Reference yield:

: 158980-57-5
3,5-dibenzyloxy-4-bromobenzoic acid tert-butyl ester

: 197804-84-5
1,1-dimethylethyl 4-[2-(benzyloxycarbonyl)phenyl]-3,5-dibenzyloxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / tetrahydrofuran; hexane / 0.25 h / -78 °C

1.2: 38 percent / trimethylborate / tetrahydrofuran; hexane / 16 h / 20 °C

2.1: 57 percent / Pd(PPh₃)4; Na₂CO₃ / dioxane / 60 h / Heating

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; sodium carbonate; In tetrahydrofuran; 1,4-dioxane; hexane; 2.1: Suzuki coupling;
DOI:10.1021/jm020018f

Reference yield:

: 67460-09-7
benzyl 2-bromobenzoate

: 158980-57-5
3,5-dibenzyloxy-4-bromobenzoic acid tert-butyl ester

: 197804-84-5
1,1-dimethylethyl 4-[2-(benzyloxycarbonyl)phenyl]-3,5-dibenzyloxybenzoate

Guidance literature:: With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; Trimethyl borate; sodium carbonate; Yield given. Multistep reaction;
DOI:10.1016/S0040-4039(97)01674-2