3’-ethyl-5'-((3-(4-fluorobenzyl)-5-heptylpyrrol-2-yl)methylene)-4'-methyl-2,2'-bipyrrole

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Chemical Name:3’-ethyl-5'-((3-(4-fluorobenzyl)-5-heptylpyrrol-2-yl)methylene)-4'-methyl-2,2'-bipyrrole
CAS No.:1450982-18-9
Molecular Formula:C₃₀H₃₆FN₃
Molecular Weight:457.634
Hs Code.:

Synonyms:3’-ethyl-5'-((3-(4-fluorobenzyl)-5-heptylpyrrol-2-yl)methylene)-4'-methyl-2,2'-bipyrrole

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Chemical Property of 3’-ethyl-5'-((3-(4-fluorobenzyl)-5-heptylpyrrol-2-yl)methylene)-4'-methyl-2,2'-bipyrrole

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Technology Process of 3’-ethyl-5'-((3-(4-fluorobenzyl)-5-heptylpyrrol-2-yl)methylene)-4'-methyl-2,2'-bipyrrole

There total 7 articles about 3’-ethyl-5'-((3-(4-fluorobenzyl)-5-heptylpyrrol-2-yl)methylene)-4'-methyl-2,2'-bipyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1450982-09-8
3‐ethyl‐4‐methyl‐1H,1′H‐[2,2′‐bipyrrole]‐5‐carbaldehyde

: 1450982-15-6
C₁₈H₂₄FN

: 1450982-18-9
3’-ethyl-5'-((3-(4-fluorobenzyl)-5-heptylpyrrol-2-yl)methylene)-4'-methyl-2,2'-bipyrrole

Guidance literature:: With hydrogenchloride; In methanol; at 20 ℃; for 2h;
DOI:10.1016/j.tet.2013.07.067

Reference yield:

: 100780-37-8
2-nitro-3-acetoxy-pentane

: 1450982-18-9
3’-ethyl-5'-((3-(4-fluorobenzyl)-5-heptylpyrrol-2-yl)methylene)-4'-methyl-2,2'-bipyrrole

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium carbonate / tetrahydrofuran; ethanol / 72 h / 20 °C

2.1: trichlorophosphate / 0 °C / Inert atmosphere

2.2: 12 h / 20 °C / Inert atmosphere

2.3: 1 h / 20 °C

3.1: pyridinium hydrobromide perbromide; pyridine / dichloromethane / 20 °C / Inert atmosphere

4.1: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water; hexane / 3 h / 100 °C

5.1: methanol; lithium hydroxide / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

6.1: hydrogenchloride / methanol / 2 h / 20 °C

With pyridine; hydrogenchloride; methanol; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; potassium carbonate; pyridinium hydrobromide perbromide; lithium hydroxide; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; hexane; dichloromethane; water; 2.1: |Vilsmeier Reaction / 4.1: |Suzuki Coupling;
DOI:10.1016/j.tet.2013.07.067

Reference yield:

: 4949-58-0
2-(ethyloxycarbonyl)-3-ethyl-4-methylpyrrole

: 1450982-18-9
3’-ethyl-5'-((3-(4-fluorobenzyl)-5-heptylpyrrol-2-yl)methylene)-4'-methyl-2,2'-bipyrrole

Guidance literature:: Multi-step reaction with 5 steps

1.1: trichlorophosphate / 0 °C / Inert atmosphere

1.2: 12 h / 20 °C / Inert atmosphere

1.3: 1 h / 20 °C

2.1: pyridinium hydrobromide perbromide; pyridine / dichloromethane / 20 °C / Inert atmosphere

3.1: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water; hexane / 3 h / 100 °C

4.1: methanol; lithium hydroxide / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

5.1: hydrogenchloride / methanol / 2 h / 20 °C

With pyridine; hydrogenchloride; methanol; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; pyridinium hydrobromide perbromide; lithium hydroxide; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; methanol; hexane; dichloromethane; water; 1.1: |Vilsmeier Reaction / 3.1: |Suzuki Coupling;
DOI:10.1016/j.tet.2013.07.067