3-hydroxymethyl-2,2,3-trimethyloxetane dihydrocinnamyl ester

Base Information

Chemical Name:3-hydroxymethyl-2,2,3-trimethyloxetane dihydrocinnamyl ester
CAS No.:845307-19-9
Molecular Formula:C₁₆H₂₂O₃
Molecular Weight:262.349
Hs Code.:

Synonyms:3-hydroxymethyl-2,2,3-trimethyloxetane dihydrocinnamyl ester

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Chemical Property of 3-hydroxymethyl-2,2,3-trimethyloxetane dihydrocinnamyl ester

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Technology Process of 3-hydroxymethyl-2,2,3-trimethyloxetane dihydrocinnamyl ester

There total 4 articles about 3-hydroxymethyl-2,2,3-trimethyloxetane dihydrocinnamyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 845307-16-6
4-tert-butyldimethylsilyloxy-3-hydroxymethyl-2,3-dimethyl-2-butanol

: 845307-19-9
3-hydroxymethyl-2,2,3-trimethyloxetane dihydrocinnamyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / potassium tert-butoxide; p-toluenesulfonyl chloride / tetrahydrofuran / 0.08 h / 20 °C

2: 55 percent / TBAF / tetrahydrofuran / 2 h / 20 °C

3: pyridine

With pyridine; potassium tert-butylate; tetrabutyl ammonium fluoride; p-toluenesulfonyl chloride; In tetrahydrofuran;
DOI:10.1021/ol047493n

Reference yield:

: benzyl 3-tert-butyldimethylsilyloxy-2-hydroxymethyl-2-methylpropionate

: 845307-19-9
3-hydroxymethyl-2,2,3-trimethyloxetane dihydrocinnamyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 42 percent / tetrahydrofuran / 0.17 h / 0 °C

2: 61 percent / potassium tert-butoxide; p-toluenesulfonyl chloride / tetrahydrofuran / 0.08 h / 20 °C

3: 55 percent / TBAF / tetrahydrofuran / 2 h / 20 °C

4: pyridine

With pyridine; potassium tert-butylate; tetrabutyl ammonium fluoride; p-toluenesulfonyl chloride; In tetrahydrofuran;
DOI:10.1021/ol047493n

Reference yield:

: 845307-17-7
3-tert-butyldimethylsilyloxymethyl-2,2,3-trimethyloxetane

: 845307-19-9
3-hydroxymethyl-2,2,3-trimethyloxetane dihydrocinnamyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / TBAF / tetrahydrofuran / 2 h / 20 °C

2: pyridine

With pyridine; tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1021/ol047493n