2-(5-bromo-2-methoxypyridin-2-yl)-5,5-dimethylcyclohex-1-enecarbaldehyde

Base Information

Chemical Name:2-(5-bromo-2-methoxypyridin-2-yl)-5,5-dimethylcyclohex-1-enecarbaldehyde
CAS No.:1621255-71-7
Molecular Formula:C₁₅H₁₈BrNO₂
Molecular Weight:324.217
Hs Code.:

Synonyms:2-(5-bromo-2-methoxypyridin-2-yl)-5,5-dimethylcyclohex-1-enecarbaldehyde

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Chemical Property of 2-(5-bromo-2-methoxypyridin-2-yl)-5,5-dimethylcyclohex-1-enecarbaldehyde

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Technology Process of 2-(5-bromo-2-methoxypyridin-2-yl)-5,5-dimethylcyclohex-1-enecarbaldehyde

There total 4 articles about 2-(5-bromo-2-methoxypyridin-2-yl)-5,5-dimethylcyclohex-1-enecarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1621256-22-1
C₁₅H₂₀BrNO₂

: 1621255-71-7
2-(5-bromo-2-methoxypyridin-2-yl)-5,5-dimethylcyclohex-1-enecarbaldehyde

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 0 - 20 ℃; for 0.5h;

Reference yield:

: 1621255-70-6
ethyl 2-(5-bromo-2-methoxypyridin-3-yl)-5,5-dimethylcyclohex-1-enecarboxylate

: 1621255-71-7
2-(5-bromo-2-methoxypyridin-2-yl)-5,5-dimethylcyclohex-1-enecarbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C

2: Dess-Martin periodane / dichloromethane / 0.5 h / 0 - 20 °C

With lithium aluminium tetrahydride; Dess-Martin periodane; In tetrahydrofuran; dichloromethane;

Reference yield:

: 1423046-22-3
C₁₇H₂₉BO₄

: 1621255-71-7
2-(5-bromo-2-methoxypyridin-2-yl)-5,5-dimethylcyclohex-1-enecarbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / water; 1,4-dioxane / 0.5 h / 120 °C / Microwave irradiation

2: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C

3: Dess-Martin periodane / dichloromethane / 0.5 h / 0 - 20 °C

With lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; Dess-Martin periodane; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; 1: |Suzuki Coupling;