C₂₄H₃₄N₂O₂Si

Base Information

Chemical Name:C₂₄H₃₄N₂O₂Si
CAS No.:1428850-30-9
Molecular Formula:C₂₄H₃₄N₂O₂Si
Molecular Weight:410.632
Hs Code.:

C<sub>24</sub>H<sub>34</sub>N<sub>2</sub>O<sub>2</sub>Si

Synonyms:C₂₄H₃₄N₂O₂Si

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Chemical Property of C₂₄H₃₄N₂O₂Si

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Technology Process of C₂₄H₃₄N₂O₂Si

There total 4 articles about C₂₄H₃₄N₂O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1428850-45-6
C₂₈H₃₈N₂O₄Si

: 1428850-30-9
C₂₄H₃₄N₂O₂Si

Guidance literature:: With morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2-methyl-but-2-ene; In tetrahydrofuran; at -5 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ja401457h

Reference yield:

: 1428850-13-8
C₂₂H₂₉IOSi

: 1428850-30-9
C₂₄H₃₄N₂O₂Si

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate; copper(l) iodide; N,N`-dimethylethylenediamine / 1,4-dioxane / 24 h / 70 °C / Inert atmosphere

2: 2-methyl-but-2-ene; morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 2 h / -5 °C / Inert atmosphere

With morpholine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2-methyl-but-2-ene; caesium carbonate; N,N`-dimethylethylenediamine; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1021/ja401457h

Reference yield:

: C₈H₁₃IO₂

: 1428850-30-9
C₂₄H₃₄N₂O₂Si

Guidance literature:: Multi-step reaction with 4 steps

1: diisobutylaluminium hydride / dichloromethane; hexane / 0.58 h / -78 °C / Inert atmosphere

2: triethylamine; dmap / 19 h / 0 - 20 °C / Inert atmosphere

3: caesium carbonate; copper(l) iodide; N,N`-dimethylethylenediamine / 1,4-dioxane / 24 h / 70 °C / Inert atmosphere

4: 2-methyl-but-2-ene; morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 2 h / -5 °C / Inert atmosphere

With morpholine; dmap; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2-methyl-but-2-ene; diisobutylaluminium hydride; caesium carbonate; triethylamine; N,N`-dimethylethylenediamine; In tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane;
DOI:10.1021/ja401457h