2-(p-chlorophenylaminosulfonylmethyl)-5-[E-(2-(p-chlorophenylsulfonyl)vinylsulfonylmethyl)]-1,3,4-thiadiazole

Base Information

• Chemical Name: 2-(p-chlorophenylaminosulfonylmethyl)-5-[E-(2-(p-chlorophenylsulfonyl)vinylsulfonylmethyl)]-1,3,4-thiadiazole
• CAS No.: 1394128-64-3
• Molecular Formula: C₁₈H₁₅Cl₂N₃O₆S₄
• Molecular Weight: 568.504

Synonyms:2-(p-chlorophenylaminosulfonylmethyl)-5-[E-(2-(p-chlorophenylsulfonyl)vinylsulfonylmethyl)]-1,3,4-thiadiazole

Chemical Property of 2-(p-chlorophenylaminosulfonylmethyl)-5-[E-(2-(p-chlorophenylsulfonyl)vinylsulfonylmethyl)]-1,3,4-thiadiazole

Chemical Property:

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Technology Process of 2-(p-chlorophenylaminosulfonylmethyl)-5-[E-(2-(p-chlorophenylsulfonyl)vinylsulfonylmethyl)]-1,3,4-thiadiazole

There total 2 articles about 2-(p-chlorophenylaminosulfonylmethyl)-5-[E-(2-(p-chlorophenylsulfonyl)vinylsulfonylmethyl)]-1,3,4-thiadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-(4-chlorophenyl)sulfonylethenesulfonylacetic acid (1155273-87-2) → 2-(p-chlorophenylaminosulfonylmethyl)-5-[E-(2-(p-chlorophenylsulfonyl)vinylsulfonylmethyl)]-1,3,4-thiadiazole (1394128-64-3)

Guidance literature:

Multi-step reaction with 2 steps

1: trichlorophosphate / Reflux

2: thiourea / tetrahydrofuran / 120 - 150 °C

With thiourea; trichlorophosphate; In tetrahydrofuran;

DOI:10.1016/j.ejmech.2012.06.014

Reference yield:

(N-4-chlorophenylsulfamoyl)acetic acid hydrazide (67542-00-1) → 2-(p-chlorophenylaminosulfonylmethyl)-5-[E-(2-(p-chlorophenylsulfonyl)vinylsulfonylmethyl)]-1,3,4-thiadiazole (1394128-64-3)

Guidance literature:

Multi-step reaction with 2 steps

1: trichlorophosphate / Reflux

2: thiourea / tetrahydrofuran / 120 - 150 °C

With thiourea; trichlorophosphate; In tetrahydrofuran;

DOI:10.1016/j.ejmech.2012.06.014

Reference yield: 73.0%

2-(p-chlorophenylaminosulfonylmethyl)-5-[E-(2-(p-chlorophenylsulfonyl)vinylsulfonylmethyl)]-1,3,4-thiadiazole (1394128-64-3) + [(p-methylphenyl)sulfonylmethyl]isonitrile (38622-91-2,36635-61-7) → 2-(p-chlorophenylaminosulfonylmethyl)-5-(4'-(p-chlorophenylsulfonyl)-1'H-pyrrol-3'-ylsulfonylmethyl)-1,3,4-thiadiazole (1394128-73-4)

Guidance literature:

With sodium hydride; In diethyl ether; dimethyl sulfoxide; at 20 ℃;

DOI:10.1016/j.ejmech.2012.06.014

upstream raw materials:

(E)-(4-chlorophenyl)sulfonylethenesulfonylacetic acid

(N-4-chlorophenylsulfamoyl)acetic acid hydrazide

Downstream raw materials:

2-(p-chlorophenylaminosulfonylmethyl)-5-(3'-(p-chlorophenylsulfonyl)-4',5'-dihydro-1'H-pyrazol-4'-ylsulfonylmethyl)-1,3,4-thiadiazole

2-(p-chlorophenylaminosulfonylmethyl)-5-(3'-(p-chlorophenylsulfonyl)-1'H-pyrazol-4'-ylsulfonylmethyl)-1,3,4-thiadiazole

2-(p-chlorophenylaminosulfonylmethyl)-5-(4'-(p-chlorophenylsulfonyl)-1'H-pyrrol-3'-ylsulfonylmethyl)-1,3,4-thiadiazole

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