Technology Process of C14H20O3
There total 7 articles about C14H20O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
diisobutylaluminium hydride;
In
dichloromethane; cyclohexane;
at -78 ℃;
for 1h;
Inert atmosphere;
DOI:10.1002/ejoc.201402096
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 14 h / 20 °C
2.1: dichloromethane / 14 h / 20 °C
3.1: sodium hexamethyldisilazane / tetrahydrofuran / 2.5 h / -78 °C / Inert atmosphere
3.2: 11.5 h / -78 - -5 °C
4.1: sodium tetrahydroborate / tetrahydrofuran; water / 18 h / 20 °C
5.1: diisobutylaluminium hydride / dichloromethane; cyclohexane / 1 h / -78 °C / Inert atmosphere
With
dmap; sodium tetrahydroborate; sodium hexamethyldisilazane; diisobutylaluminium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
tetrahydrofuran; dichloromethane; cyclohexane; water;
2.1: |Wittig Olefination;
DOI:10.1002/ejoc.201402096
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: dichloromethane / 14 h / 20 °C
2.1: sodium hexamethyldisilazane / tetrahydrofuran / 2.5 h / -78 °C / Inert atmosphere
2.2: 11.5 h / -78 - -5 °C
3.1: sodium tetrahydroborate / tetrahydrofuran; water / 18 h / 20 °C
4.1: diisobutylaluminium hydride / dichloromethane; cyclohexane / 1 h / -78 °C / Inert atmosphere
With
sodium tetrahydroborate; sodium hexamethyldisilazane; diisobutylaluminium hydride;
In
tetrahydrofuran; dichloromethane; cyclohexane; water;
1.1: |Wittig Olefination;
DOI:10.1002/ejoc.201402096
