ethyl 2-[4-(2-ethoxy-2-oxoethyl)-3,5-dioxo-1,2,4-thiadiazolidin-2-yl]-3-phenylpropanoate

Base Information

Chemical Name:ethyl 2-[4-(2-ethoxy-2-oxoethyl)-3,5-dioxo-1,2,4-thiadiazolidin-2-yl]-3-phenylpropanoate
CAS No.:1452185-37-3
Molecular Formula:C₁₇H₂₀N₂O₆S
Molecular Weight:380.422
Hs Code.:

Synonyms:ethyl 2-[4-(2-ethoxy-2-oxoethyl)-3,5-dioxo-1,2,4-thiadiazolidin-2-yl]-3-phenylpropanoate

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Chemical Property of ethyl 2-[4-(2-ethoxy-2-oxoethyl)-3,5-dioxo-1,2,4-thiadiazolidin-2-yl]-3-phenylpropanoate

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Technology Process of ethyl 2-[4-(2-ethoxy-2-oxoethyl)-3,5-dioxo-1,2,4-thiadiazolidin-2-yl]-3-phenylpropanoate

There total 3 articles about ethyl 2-[4-(2-ethoxy-2-oxoethyl)-3,5-dioxo-1,2,4-thiadiazolidin-2-yl]-3-phenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 37682-80-7
2-isocyanato-3-phenyl-propionic acid ethyl ester

: C₅H₇Cl₂NO₂S

: 1452185-37-3
ethyl 2-[4-(2-ethoxy-2-oxoethyl)-3,5-dioxo-1,2,4-thiadiazolidin-2-yl]-3-phenylpropanoate

Guidance literature:: 2-isocyanato-3-phenyl-propionic acid ethyl ester; C₅H₇Cl₂NO₂S; at -10 - 20 ℃; for 18h; Inert atmosphere;

With water; In n-heptane; Solvent; Concentration;

Reference yield:

: 3182-93-2
(L)-phenylalanine ethyl ester hydrochloride

: 1452185-37-3
ethyl 2-[4-(2-ethoxy-2-oxoethyl)-3,5-dioxo-1,2,4-thiadiazolidin-2-yl]-3-phenylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydrogencarbonate / dichloromethane; water / 0.5 h / 0 °C

1.2: 2 h / 0 - 20 °C

2.1: 18 h / -10 - 20 °C / Inert atmosphere

With sodium hydrogencarbonate; In dichloromethane; water;

Reference yield:

: 24066-82-8
ethyl 2-isothiocyanatoacetate

: 1452185-37-3
ethyl 2-[4-(2-ethoxy-2-oxoethyl)-3,5-dioxo-1,2,4-thiadiazolidin-2-yl]-3-phenylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuryl dichloride / 3 h / -10 °C / Inert atmosphere

2: 18 h / -10 - 20 °C / Inert atmosphere

With sulfuryl dichloride;