trifluoro-methanesulfonic acid 2-(1-benzenesulfonyl-1H-indol-3-yl)-ethyl ester

Base Information

Chemical Name:trifluoro-methanesulfonic acid 2-(1-benzenesulfonyl-1H-indol-3-yl)-ethyl ester
CAS No.:868632-12-6
Molecular Formula:C₁₇H₁₄F₃NO₅S₂
Molecular Weight:433.429
Hs Code.:

trifluoro-methanesulfonic acid 2-(1-benzenesulfonyl-1<i>H</i>-indol-3-yl)-ethyl ester

Synonyms:trifluoro-methanesulfonic acid 2-(1-benzenesulfonyl-1H-indol-3-yl)-ethyl ester

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Chemical Property of trifluoro-methanesulfonic acid 2-(1-benzenesulfonyl-1H-indol-3-yl)-ethyl ester

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Technology Process of trifluoro-methanesulfonic acid 2-(1-benzenesulfonyl-1H-indol-3-yl)-ethyl ester

There total 1 articles about trifluoro-methanesulfonic acid 2-(1-benzenesulfonyl-1H-indol-3-yl)-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 358-23-6
trifluoromethylsulfonic anhydride

: 99655-69-3
3-(2-hydroxyethyl)-1-(benzenesulfonyl)indole

: 868632-12-6
trifluoro-methanesulfonic acid 2-(1-benzenesulfonyl-1H-indol-3-yl)-ethyl ester

Guidance literature:: With 2,6-di-tert-butyl-4-methylpyridine; In dichloromethane; at 20 ℃; for 0.333333h;
DOI:10.1021/jo051454n

Reference yield:

: 868632-12-6
trifluoro-methanesulfonic acid 2-(1-benzenesulfonyl-1H-indol-3-yl)-ethyl ester

: 2-O-(5-aminopentyl)-1-O-[2-(indol-3-yl)ethyl]catechol

Guidance literature:: Multi-step reaction with 3 steps

1: 37 percent / sodium hydride / diethyl ether / 4 h / 0 - 20 °C

2: 100 percent / water; triphenylphosphine / tetrahydrofuran / 5 h / Heating

3: 95 percent / sodium hydroxide / methanol; H₂O / 20 h / Heating

With sodium hydroxide; water; sodium hydride; triphenylphosphine; In tetrahydrofuran; methanol; diethyl ether; water; 2: Staudinger reduction;
DOI:10.1021/ol061488x

Reference yield:

: 868632-12-6
trifluoro-methanesulfonic acid 2-(1-benzenesulfonyl-1H-indol-3-yl)-ethyl ester

: 913941-80-7
2-O-(5-aminopentyl)-1-O-[2-[1-(benzenesulfonyl)indol-3-yl]ethyl]catechol

Guidance literature:: Multi-step reaction with 2 steps

1: 37 percent / sodium hydride / diethyl ether / 4 h / 0 - 20 °C

2: 100 percent / water; triphenylphosphine / tetrahydrofuran / 5 h / Heating

With water; sodium hydride; triphenylphosphine; In tetrahydrofuran; diethyl ether; 2: Staudinger reduction;
DOI:10.1021/ol061488x