1,2-diphenylethyl diphenylphosphinate

Base Information

Chemical Name:1,2-diphenylethyl diphenylphosphinate
CAS No.:19639-46-4
Molecular Formula:C₂₆H₂₃O₂P
Molecular Weight:398.441
Hs Code.:

Synonyms:1,2-diphenylethyl diphenylphosphinate

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Chemical Property of 1,2-diphenylethyl diphenylphosphinate

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Technology Process of 1,2-diphenylethyl diphenylphosphinate

There total 2 articles about 1,2-diphenylethyl diphenylphosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 5773-56-8,614-29-9
1,2-Diphenylethanol

: 1499-21-4
Diphenylphosphinic chloride

: 19639-46-4
1,2-diphenylethyl diphenylphosphinate

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/anie.202105895

Reference yield:

: 1707-03-5
diphenyl-phosphinic acid

: 103-29-7
1,1'-(1,2-ethanediyl)bisbenzene

: 19639-46-4
1,2-diphenylethyl diphenylphosphinate

Guidance literature:: With di-tert-butyl peroxide; cetyltrimethylammonim bromide; at 120 ℃; for 10h; Inert atmosphere; Schlenk technique;
DOI:10.1039/c8ob02772b

Reference yield: 51.0%

: 19639-46-4
1,2-diphenylethyl diphenylphosphinate

: 103-29-7
1,1'-(1,2-ethanediyl)bisbenzene

Guidance literature:: With 2-(4-butoxyphenyl)-1H-benzo[de]isoquinoline-1,3(2H)-dione; tert-butylammonium hexafluorophosphate(V); In acetonitrile; at 20 ℃; for 36h; Inert atmosphere; Electrochemical reaction; Irradiation;
DOI:10.1002/anie.202105895