Technology Process of 1,1,2,2-Tetraphenyl-trisilane
There total 6 articles about 1,1,2,2-Tetraphenyl-trisilane which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 1.) triflic acid, 2.) LiF / 1.) toluene, rt, 15 h, 2.) toluene, Et2O, reflux, 20 h
2: 94 percent / LiAlH4 / diethyl ether / 48 h / Ambient temperature
3: 1.) triflic acid, 2.) LiF / 1.) toluene, 3 h, 2.) toluene, Et2O, reflux, 8 h
4: 91 percent / LiAlH4 / diethyl ether / 48 h / Ambient temperature
5: 1.) triflic acid, 2.) LiF / 1.) toluene, 4 h, 2.) toluene, Et2O, 20 h
6: 83 percent / LiAlH4 / diethyl ether / 48 h / Ambient temperature
With
lithium aluminium tetrahydride; trifluorormethanesulfonic acid; lithium fluoride;
In
diethyl ether;
DOI:10.1016/S0022-328X(96)06543-6
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) triflic acid, 2.) LiF / 1.) toluene, 4 h, 2.) toluene, Et2O, 20 h
2: 83 percent / LiAlH4 / diethyl ether / 48 h / Ambient temperature
With
lithium aluminium tetrahydride; trifluorormethanesulfonic acid; lithium fluoride;
In
diethyl ether;
DOI:10.1016/S0022-328X(96)06543-6
