Technology Process of C41H50O8
There total 1 articles about C41H50O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C41H52O9;
With
1,1,1,2-tetrachloro-2-methylpropane; triethylamine;
In
toluene;
at 20 ℃;
for 3h;
With
dmap;
In
toluene;
at 20 ℃;
for 15h;
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
methanol;
at 20 ℃;
for 4h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: trifluoroacetic anhydride; 18-crown-6 ether; tetrabutylammonium nitrate / dichloromethane / 1 h / 20 °C
2: nickel chloride monohydrate; sodium tetrahydroborate / methanol; tetrahydrofuran / 4 °C
3: triethylamine / dichloromethane / 4 h / 20 °C
4: palladium on activated charcoal; hydrogen / ethanol / 4 h / 20 °C
With
sodium tetrahydroborate; 18-crown-6 ether; nickel chloride monohydrate; palladium on activated charcoal; hydrogen; tetrabutylammonium nitrate; triethylamine; trifluoroacetic anhydride;
In
tetrahydrofuran; methanol; ethanol; dichloromethane;
DOI:10.1016/j.bmc.2013.03.013