(S)-4-[(1R,2R)-2-(tert-butyl-diphenyl-silanyloxy)-1-(3,4,5-trifluorophenyl)propyl]-2-hydroxy-6-methylmorpholin-3-one

Base Information

Chemical Name:(S)-4-[(1R,2R)-2-(tert-butyl-diphenyl-silanyloxy)-1-(3,4,5-trifluorophenyl)propyl]-2-hydroxy-6-methylmorpholin-3-one
CAS No.:937399-75-2
Molecular Formula:C₃₀H₃₄F₃NO₄Si
Molecular Weight:557.685
Hs Code.:

Synonyms:(S)-4-[(1R,2R)-2-(tert-butyl-diphenyl-silanyloxy)-1-(3,4,5-trifluorophenyl)propyl]-2-hydroxy-6-methylmorpholin-3-one

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Chemical Property of (S)-4-[(1R,2R)-2-(tert-butyl-diphenyl-silanyloxy)-1-(3,4,5-trifluorophenyl)propyl]-2-hydroxy-6-methylmorpholin-3-one

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Technology Process of (S)-4-[(1R,2R)-2-(tert-butyl-diphenyl-silanyloxy)-1-(3,4,5-trifluorophenyl)propyl]-2-hydroxy-6-methylmorpholin-3-one

There total 1 articles about (S)-4-[(1R,2R)-2-(tert-butyl-diphenyl-silanyloxy)-1-(3,4,5-trifluorophenyl)propyl]-2-hydroxy-6-methylmorpholin-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 937399-74-1
(S)-4-[(1R,2R)-2-(tert-butyl-diphenyl-silanyloxy)-1-(3,4,5-trifluorophenyl)propyl]-6-methylmorpholine-2,3-dione

: 937399-75-2
(S)-4-[(1R,2R)-2-(tert-butyl-diphenyl-silanyloxy)-1-(3,4,5-trifluorophenyl)propyl]-2-hydroxy-6-methylmorpholin-3-one

Guidance literature:: (S)-4-[(1R,2R)-2-(tert-butyl-diphenyl-silanyloxy)-1-(3,4,5-trifluorophenyl)propyl]-6-methylmorpholine-2,3-dione; With L-Selectride; In tetrahydrofuran; at -20 ℃; for 0.5h;

With sodium hydroxide; water; dihydrogen peroxide; In tetrahydrofuran; at 0 ℃; for 1h;

Reference yield:

: 937399-75-2
(S)-4-[(1R,2R)-2-(tert-butyl-diphenyl-silanyloxy)-1-(3,4,5-trifluorophenyl)propyl]-2-hydroxy-6-methylmorpholin-3-one

: 958228-07-4
3-methoxy-4-(3-methyl-1H-[1,2,4]triazol-1-yl)benzaldehyde

: C₄₁H₄₃F₃N₄O₄Si

Guidance literature:: (S)-4-[(1R,2R)-2-(tert-butyl-diphenyl-silanyloxy)-1-(3,4,5-trifluorophenyl)propyl]-2-hydroxy-6-methylmorpholin-3-one; With triphenylphosphine hydrobromide; In acetonitrile; for 1h; Heating / reflux;

3-methoxy-4-(3-methyl-1H-[1,2,4]triazol-1-yl)benzaldehyde; With triethylamine; In ethanol; at 70 - 80 ℃; for 1h;

Reference yield:

: 870837-18-6
3-methoxy-4-(4-methyl-1H-imidazol-1-yl)benzaldehyde

: 937399-75-2
(S)-4-[(1R,2R)-2-(tert-butyl-diphenyl-silanyloxy)-1-(3,4,5-trifluorophenyl)propyl]-2-hydroxy-6-methylmorpholin-3-one

: C₄₂H₄₄F₃N₃O₄Si

Guidance literature:: (S)-4-[(1R,2R)-2-(tert-butyl-diphenyl-silanyloxy)-1-(3,4,5-trifluorophenyl)propyl]-2-hydroxy-6-methylmorpholin-3-one; With triphenylphosphine hydrobromide; In acetonitrile; for 1h; Heating / reflux;

3-methoxy-4-(4-methyl-1H-imidazol-1-yl)benzaldehyde; With triethylamine; In ethanol; at 20 ℃;