(methylcyclopentadienyl)2V2(μ-η2-S2)(μ-η1-4-phenyl-1,2,4-triazoline-3,5-dione)2 * dichloromethane

Base Information

Chemical Name:(methylcyclopentadienyl)2V2(μ-η2-S2)(μ-η1-4-phenyl-1,2,4-triazoline-3,5-dione)2 * dichloromethane
CAS No.:92641-97-9
Molecular Formula:CH₂Cl₂*C₂₈H₂₄N₆O₄S₂V₂
Molecular Weight:759.484
Hs Code.:

Synonyms:(methylcyclopentadienyl)2V2(μ-η2-S2)(μ-η1-4-phenyl-1,2,4-triazoline-3,5-dione)2 * dichloromethane

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Chemical Property of (methylcyclopentadienyl)2V2(μ-η2-S2)(μ-η1-4-phenyl-1,2,4-triazoline-3,5-dione)2 * dichloromethane

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Technology Process of (methylcyclopentadienyl)2V2(μ-η2-S2)(μ-η1-4-phenyl-1,2,4-triazoline-3,5-dione)2 * dichloromethane

There total 3 articles about (methylcyclopentadienyl)2V2(μ-η2-S2)(μ-η1-4-phenyl-1,2,4-triazoline-3,5-dione)2 * dichloromethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.7%

: 4233-33-4
4-Phenyl-1,2,4-triazolidine-3,5-dione

: (η5-methylcyclopentadienyl)2V2S4

: 92641-96-8
(methylcyclopentadienyl)2V2(μ-S)2(μ-η1-4-phenyl-1,2,4-triazoline-3,5-dione)

: 92641-97-9
(methylcyclopentadienyl)2V2(μ-η2-S2)(μ-η1-4-phenyl-1,2,4-triazoline-3,5-dione)2 * dichloromethane

: 92641-95-7
(methylcyclopentadienyl)2V2(μ-S)(μ-η2-S2)(μ-η1-4-phenyl-1,2,4-triazoline-3,5-dione)

: 82978-84-5
(CH₃C₅H₄)2V₂S₅

Guidance literature:: With CH₂Cl₂; In tetrahydrofuran; under N2, educts dissolved in THF, reacted for 1 h; filtered through Celite, evapd., extd. with CH2Cl2, chromd. (SiO2, CH2Cl2, acetone); elem. anal.;
DOI:10.1021/ja00337a025

Reference yield: 42.0%

: 4233-33-4
4-Phenyl-1,2,4-triazolidine-3,5-dione

: 92641-96-8
(methylcyclopentadienyl)2V2(μ-S)2(μ-η1-4-phenyl-1,2,4-triazoline-3,5-dione)

: 92641-97-9
(methylcyclopentadienyl)2V2(μ-η2-S2)(μ-η1-4-phenyl-1,2,4-triazoline-3,5-dione)2 * dichloromethane

: 92641-95-7
(methylcyclopentadienyl)2V2(μ-S)(μ-η2-S2)(μ-η1-4-phenyl-1,2,4-triazoline-3,5-dione)

Guidance literature:: With CH₂Cl₂; In tetrahydrofuran; under N2, soln. of educts in THF heated to reflux for 2.5 h, cooled; filtered, evapd., extd. with toluene, concd., cooled to -25°C, filtered, recrystd. from CH2Cl2/MeOH and CH2Cl2/hexane; combined filtrates filtered through SiO2 plug; elem. anal.;
DOI:10.1021/ja00337a025