C₂₈H₄₇NO₅Si₂

Base Information

Chemical Name:C₂₈H₄₇NO₅Si₂
CAS No.:1410805-39-8
Molecular Formula:C₂₈H₄₇NO₅Si₂
Molecular Weight:533.856
Hs Code.:

C<sub>28</sub>H<sub>47</sub>NO<sub>5</sub>Si<sub>2</sub>

Synonyms:C₂₈H₄₇NO₅Si₂

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Chemical Property of C₂₈H₄₇NO₅Si₂

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Technology Process of C₂₈H₄₇NO₅Si₂

There total 6 articles about C₂₈H₄₇NO₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 102191-92-4
tert-butyldimethylsiloxyacetaldehyde

: 1410805-39-8
C₂₈H₄₇NO₅Si₂

Guidance literature:: Multi-step reaction with 6 steps

1: dimethyl zinc(II); ((2S,2'S)-((2-hydroxy-5-methyl-1,3-phenylene)bis(methylene))bis(pyrrolidine-1,2-diyl))bis(diphenylmethanol) / toluene / 36 h / 20 °C / Inert atmosphere

2: 1H-imidazole / N,N-dimethyl-formamide / 3.5 h / 0 °C / Inert atmosphere

3: potassium hydrogencarbonate; N-chloro-succinimide / ethyl acetate / 120 h / 20 - 48 °C / Inert atmosphere

4: diisobutylaluminium hydride / hexane; toluene / 2 h / -78 °C / Inert atmosphere

5: sulfur trioxide pyridine complex; N-ethyl-N,N-diisopropylamine / dichloromethane; dimethyl sulfoxide / 1 h / 0 °C / Inert atmosphere

6: pentane; diethyl ether / 1 h / -110 - -78 °C / Inert atmosphere

With 1H-imidazole; N-chloro-succinimide; dimethyl zinc(II); sulfur trioxide pyridine complex; diisobutylaluminium hydride; potassium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; ((2S,2'S)-((2-hydroxy-5-methyl-1,3-phenylene)bis(methylene))bis(pyrrolidine-1,2-diyl))bis(diphenylmethanol); In diethyl ether; hexane; dichloromethane; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; toluene; pentane;
DOI:10.1021/ol302691j

Reference yield:

: 1410805-35-4
C₁₂H₂₂O₄Si

: 1410805-39-8
C₂₈H₄₇NO₅Si₂

Guidance literature:: Multi-step reaction with 5 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 3.5 h / 0 °C / Inert atmosphere

2: potassium hydrogencarbonate; N-chloro-succinimide / ethyl acetate / 120 h / 20 - 48 °C / Inert atmosphere

3: diisobutylaluminium hydride / hexane; toluene / 2 h / -78 °C / Inert atmosphere

4: sulfur trioxide pyridine complex; N-ethyl-N,N-diisopropylamine / dichloromethane; dimethyl sulfoxide / 1 h / 0 °C / Inert atmosphere

5: pentane; diethyl ether / 1 h / -110 - -78 °C / Inert atmosphere

With 1H-imidazole; N-chloro-succinimide; sulfur trioxide pyridine complex; diisobutylaluminium hydride; potassium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; In diethyl ether; hexane; dichloromethane; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; toluene; pentane;
DOI:10.1021/ol302691j

Reference yield:

: 1410805-36-5
C₂₆H₄₃NO₆Si₂

: 1410805-39-8
C₂₈H₄₇NO₅Si₂

Guidance literature:: Multi-step reaction with 3 steps

1: diisobutylaluminium hydride / hexane; toluene / 2 h / -78 °C / Inert atmosphere

2: sulfur trioxide pyridine complex; N-ethyl-N,N-diisopropylamine / dichloromethane; dimethyl sulfoxide / 1 h / 0 °C / Inert atmosphere

3: pentane; diethyl ether / 1 h / -110 - -78 °C / Inert atmosphere

With sulfur trioxide pyridine complex; diisobutylaluminium hydride; N-ethyl-N,N-diisopropylamine; In diethyl ether; hexane; dichloromethane; dimethyl sulfoxide; toluene; pentane;
DOI:10.1021/ol302691j