((CH₃)5C₅)RuH₂(P(C₃H₇)3)Ge(C₆H₂(CH₃)3)2⁽¹⁺⁾*CF₃SO₃^(1-)=[((CH₃)5C₅)RuH₂(P(C₃H₇)3)Ge(C₆H₂(CH₃)3)2][CF₃SO₃]

Base Information

• Chemical Name: ((CH₃)5C₅)RuH₂(P(C₃H₇)3)Ge(C₆H₂(CH₃)3)2⁽¹⁺⁾*CF₃SO₃^(1-)=[((CH₃)5C₅)RuH₂(P(C₃H₇)3)Ge(C₆H₂(CH₃)3)2][CF₃SO₃]
• CAS No.: 1388694-35-6
• Molecular Formula: CF₃O₃S*C₃₇H₆₀GePRu
• Molecular Weight: 858.588

Synonyms:((CH₃)5C₅)RuH₂(P(C₃H₇)3)Ge(C₆H₂(CH₃)3)2⁽¹⁺⁾*CF₃SO₃^(1-)=[((CH₃)5C₅)RuH₂(P(C₃H₇)3)Ge(C₆H₂(CH₃)3)2][CF₃SO₃]

Chemical Property of ((CH₃)5C₅)RuH₂(P(C₃H₇)3)Ge(C₆H₂(CH₃)3)2⁽¹⁺⁾*CF₃SO₃^(1-)=[((CH₃)5C₅)RuH₂(P(C₃H₇)3)Ge(C₆H₂(CH₃)3)2][CF₃SO₃]

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Technology Process of ((CH₃)5C₅)RuH₂(P(C₃H₇)3)Ge(C₆H₂(CH₃)3)2⁽¹⁺⁾*CF₃SO₃^(1-)=[((CH₃)5C₅)RuH₂(P(C₃H₇)3)Ge(C₆H₂(CH₃)3)2][CF₃SO₃]

There total 2 articles about ((CH₃)5C₅)RuH₂(P(C₃H₇)3)Ge(C₆H₂(CH₃)3)2⁽¹⁺⁾*CF₃SO₃^(1-)=[((CH₃)5C₅)RuH₂(P(C₃H₇)3)Ge(C₆H₂(CH₃)3)2][CF₃SO₃] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

[H(OEt2)2][B(C6F5)4] + ((CH3)5C5)RuH(P(C3H7)3)Ge(C6H2(CH3)3)2 (1388694-38-9) → ((CH3)5C5)RuH2(P(C3H7)3)Ge(C6H2(CH3)3)2(1+)*CF3SO3(1-)=[((CH3)5C5)RuH2(P(C3H7)3)Ge(C6H2(CH3)3)2][CF3SO3] (1388694-35-6)

Guidance literature:

In further solvent(s); 1:1 mixt. in C6D5Br heated at 60°C for 24 h R; NM;

DOI:10.1039/c2cc32840b

Reference yield:

bis(2,4,6-trimethylphenyl)germane (72876-19-8) + [Ru(η5-pentamethylcyclopentadienyl)(OTf)(P(i-Pr)3)] (1335244-30-8) → ((CH3)5C5)RuH2(P(C3H7)3)Ge(C6H2(CH3)3)2(1+)*CF3SO3(1-)=[((CH3)5C5)RuH2(P(C3H7)3)Ge(C6H2(CH3)3)2][CF3SO3] (1388694-35-6)

Guidance literature:

In fluorobenzene; Ge compd. and Ru compd. (1.7:1 molar ratio); Organometallics, 2011, vol.30, pp. 5524-5531; pptd. (pentane), septd., dried (vac.);

DOI:10.1039/c2cc32840b

Reference yield: 92.0%

((CH3)5C5)RuH2(P(C3H7)3)Ge(C6H2(CH3)3)2(1+)*CF3SO3(1-)=[((CH3)5C5)RuH2(P(C3H7)3)Ge(C6H2(CH3)3)2][CF3SO3] (1388694-35-6) → ((CH3)5C5)RuH(P(C3H7)3)Ge(C6H2(CH3)3)2 (1388694-38-9)

Guidance literature:

With N,N-p-dimethylaminopyridine; In fluorobenzene; Ge compd. treated with DMAP (1:1 molar ratio); evapd., extd. (pentane), crystd.;

DOI:10.1039/c2cc32840b

upstream raw materials:

((CH₃)5C₅)RuH(P(C₃H₇)3)Ge(C₆H₂(CH₃)3)2

bis(2,4,6-trimethylphenyl)germane

[Ru(η5-pentamethylcyclopentadienyl)(OTf)(P(i-Pr)3)]

Downstream raw materials:

((CH₃)5C₅)RuH(P(C₃H₇)3)Ge(C₆H₂(CH₃)3)2

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