Technology Process of C33H34N2O5S
There total 4 articles about C33H34N2O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C15H27NO2Sn;
With
n-butyllithium;
In
tetrahydrofuran; hexane;
at 20 ℃;
for 0.25h;
With
zinc(II) chloride;
In
tetrahydrofuran; hexane;
for 0.25h;
C21H16BrNO3S;
With
palladium diacetate; ruphos;
In
tetrahydrofuran; hexane;
for 16h;
DOI:10.1002/chem.201103605
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium carbonate; lithium bromide / N,N-dimethyl-formamide / 0.75 h / 110 °C
2.1: potassium carbonate / N,N-dimethyl-formamide / 1.5 h / 90 °C
3.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / 20 °C
3.2: 0.25 h
3.3: 16 h
With
n-butyllithium; lithium carbonate; potassium carbonate; lithium bromide;
In
tetrahydrofuran; hexane; N,N-dimethyl-formamide;
DOI:10.1002/chem.201103605
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 1.5 h / 90 °C
2.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / 20 °C
2.2: 0.25 h
2.3: 16 h
With
n-butyllithium; potassium carbonate;
In
tetrahydrofuran; hexane; N,N-dimethyl-formamide;
DOI:10.1002/chem.201103605