rac-(2S,3S)-5-allyl-6-hydroxy-2-(3,4,5-trimethoxyphenyl)-3-methyl-2,3-dihydrobenzofuran

Base Information

Chemical Name:rac-(2S,3S)-5-allyl-6-hydroxy-2-(3,4,5-trimethoxyphenyl)-3-methyl-2,3-dihydrobenzofuran
CAS No.:104832-92-0
Molecular Formula:C₂₁H₂₄O₅
Molecular Weight:356.419
Hs Code.:

Synonyms:rac-(2S,3S)-5-allyl-6-hydroxy-2-(3,4,5-trimethoxyphenyl)-3-methyl-2,3-dihydrobenzofuran

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Chemical Property of rac-(2S,3S)-5-allyl-6-hydroxy-2-(3,4,5-trimethoxyphenyl)-3-methyl-2,3-dihydrobenzofuran

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Technology Process of rac-(2S,3S)-5-allyl-6-hydroxy-2-(3,4,5-trimethoxyphenyl)-3-methyl-2,3-dihydrobenzofuran

There total 5 articles about rac-(2S,3S)-5-allyl-6-hydroxy-2-(3,4,5-trimethoxyphenyl)-3-methyl-2,3-dihydrobenzofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 104761-74-2
3,4,5-trimethoxycinnamyl 3-(allyloxy)phenyl ether

: 104832-92-0
rac-(2S,3S)-5-allyl-6-hydroxy-2-(3,4,5-trimethoxyphenyl)-3-methyl-2,3-dihydrobenzofuran

Guidance literature:: With N,N-diethylaniline; at 225 ℃; for 13h;
DOI:10.1021/jm00384a023

Reference yield:

: 1616-51-9
3-allyloxyphenol

: 104832-92-0
rac-(2S,3S)-5-allyl-6-hydroxy-2-(3,4,5-trimethoxyphenyl)-3-methyl-2,3-dihydrobenzofuran

Guidance literature:: Multi-step reaction with 2 steps

1: 17 percent / diethyl azodicarboxylate, triphenylphosphine / tetrahydrofuran / Ambient temperature

2: 24 percent / diethylaniline / 13 h / 225 °C

With triphenylphosphine; N,N-diethylaniline; diethylazodicarboxylate; In tetrahydrofuran;
DOI:10.1021/jm00384a023

Reference yield:

: 1504-56-9
(E)-3-(3,4,5-trimethoxyphenyl)prop-2-en-1-ol

: 104832-92-0
rac-(2S,3S)-5-allyl-6-hydroxy-2-(3,4,5-trimethoxyphenyl)-3-methyl-2,3-dihydrobenzofuran

Guidance literature:: Multi-step reaction with 2 steps

1: 17 percent / diethyl azodicarboxylate, triphenylphosphine / tetrahydrofuran / Ambient temperature

2: 24 percent / diethylaniline / 13 h / 225 °C

With triphenylphosphine; N,N-diethylaniline; diethylazodicarboxylate; In tetrahydrofuran;
DOI:10.1021/jm00384a023