ethyl 1-(2-phenylethenyl)-1,2,6,7,8,8a-hexahydro-4-isoquinolinecarboxylate

Base Information

Chemical Name:ethyl 1-(2-phenylethenyl)-1,2,6,7,8,8a-hexahydro-4-isoquinolinecarboxylate
CAS No.:909032-51-5
Molecular Formula:C₂₀H₂₃NO₂
Molecular Weight:309.408
Hs Code.:

Synonyms:ethyl 1-(2-phenylethenyl)-1,2,6,7,8,8a-hexahydro-4-isoquinolinecarboxylate

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Chemical Property of ethyl 1-(2-phenylethenyl)-1,2,6,7,8,8a-hexahydro-4-isoquinolinecarboxylate

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Technology Process of ethyl 1-(2-phenylethenyl)-1,2,6,7,8,8a-hexahydro-4-isoquinolinecarboxylate

There total 4 articles about ethyl 1-(2-phenylethenyl)-1,2,6,7,8,8a-hexahydro-4-isoquinolinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 1125-99-1
1-(1-Cyclohexen-1-yl)pyrrolidine

: 182418-55-9
1-(ethoxycarbonyl)-6-phenyl-3-azahexa-1,3,5-triene

: 909032-51-5
ethyl 1-(2-phenylethenyl)-1,2,6,7,8,8a-hexahydro-4-isoquinolinecarboxylate

Guidance literature:: In chloroform; at 20 ℃; for 18h;
DOI:10.1016/j.tet.2006.05.073

Reference yield:

: 4-(ethoxycarbonyl)-1,1,1-trimethyl-2-aza-1-λ⁵-phosphabuta-1,3-diene

: 909032-51-5
ethyl 1-(2-phenylethenyl)-1,2,6,7,8,8a-hexahydro-4-isoquinolinecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent Spectr_. / CHCl₃ / 1 h / 20 °C

2: 42 percent / CHCl₃ / 18 h / 20 °C

In chloroform; 1: aza-Wittig reaction;
DOI:10.1016/j.tet.2006.05.073

Reference yield:

: 14371-10-9
(E)-3-phenylpropenal

: 909032-51-5
ethyl 1-(2-phenylethenyl)-1,2,6,7,8,8a-hexahydro-4-isoquinolinecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent Spectr_. / CHCl₃ / 1 h / 20 °C

2: 42 percent / CHCl₃ / 18 h / 20 °C

In chloroform; 1: aza-Wittig reaction;
DOI:10.1016/j.tet.2006.05.073