3-(dichloroamino)-N-(2-(2-(2-methoxyethoxy)ethoxy)ethyl)-N,N,3-trimethylbutan-1-aminium 4-methylbenzenesulfonate

Base Information

Chemical Name:3-(dichloroamino)-N-(2-(2-(2-methoxyethoxy)ethoxy)ethyl)-N,N,3-trimethylbutan-1-aminium 4-methylbenzenesulfonate
CAS No.:1373433-79-4
Molecular Formula:C₇H₇O₃S*C₁₄H₃₁Cl₂N₂O₃
Molecular Weight:517.515
Hs Code.:

Synonyms:3-(dichloroamino)-N-(2-(2-(2-methoxyethoxy)ethoxy)ethyl)-N,N,3-trimethylbutan-1-aminium 4-methylbenzenesulfonate

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Chemical Property of 3-(dichloroamino)-N-(2-(2-(2-methoxyethoxy)ethoxy)ethyl)-N,N,3-trimethylbutan-1-aminium 4-methylbenzenesulfonate

Chemical Property:

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Technology Process of 3-(dichloroamino)-N-(2-(2-(2-methoxyethoxy)ethoxy)ethyl)-N,N,3-trimethylbutan-1-aminium 4-methylbenzenesulfonate

There total 8 articles about 3-(dichloroamino)-N-(2-(2-(2-methoxyethoxy)ethoxy)ethyl)-N,N,3-trimethylbutan-1-aminium 4-methylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1373433-83-0
3-amino-N-(2-(2-(2-methoxyethoxy)ethoxy)ethyl)-N,N,3-trimethylbutan-1-aminium 4-methylbenzenesulfonate

: 1373433-79-4
3-(dichloroamino)-N-(2-(2-(2-methoxyethoxy)ethoxy)ethyl)-N,N,3-trimethylbutan-1-aminium 4-methylbenzenesulfonate

Guidance literature:: With tert-butylhypochlorite; In methanol; at 0 ℃; for 0.75h;

Reference yield:

: 933738-55-7
N,N-3-trimethylbutane-1,3-diamine

: 1373433-79-4
3-(dichloroamino)-N-(2-(2-(2-methoxyethoxy)ethoxy)ethyl)-N,N,3-trimethylbutan-1-aminium 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / 17 h / 20 °C

2: 45 °C

3: hydrogen / palladium 10% on activated carbon / methanol / 18 h / 988.07 Torr

4: tert-butylhypochlorite / methanol / 0.75 h / 0 °C

With tert-butylhypochlorite; hydrogen; palladium 10% on activated carbon; In tetrahydrofuran; methanol;

Reference yield:

: 105090-72-0
3-azido-3-methylbutanoic acid

: 1373433-79-4
3-(dichloroamino)-N-(2-(2-(2-methoxyethoxy)ethoxy)ethyl)-N,N,3-trimethylbutan-1-aminium 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 7 steps

1.1: thionyl chloride / 1,2-dichloro-ethane / 2 h / 50 °C

2.1: dichloromethane; water / 1 h / 0 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 22 h / 20 - 70 °C / Cooling with ice

3.2: 0.33 h / Cooling with ice

3.3: 0.33 h

4.1: tetrahydrofuran / 17 h / 20 °C

5.1: 45 °C

6.1: hydrogen / palladium 10% on activated carbon / methanol / 18 h / 988.07 Torr

7.1: tert-butylhypochlorite / methanol / 0.75 h / 0 °C

With lithium aluminium tetrahydride; thionyl chloride; tert-butylhypochlorite; hydrogen; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane; water; 1,2-dichloro-ethane;