(1S, 2R)-1-(4-hydroxy-3-methoxyphenyl)-2-(2-methoxyphenoxy)propane-1,3-diol

Base Information

• Chemical Name: (1S, 2R)-1-(4-hydroxy-3-methoxyphenyl)-2-(2-methoxyphenoxy)propane-1,3-diol
• CAS No.: 1189197-76-9
• Molecular Formula: C₁₇H₂₀O₆
• Molecular Weight: 320.342

Synonyms:(1S, 2R)-1-(4-hydroxy-3-methoxyphenyl)-2-(2-methoxyphenoxy)propane-1,3-diol

Chemical Property of (1S, 2R)-1-(4-hydroxy-3-methoxyphenyl)-2-(2-methoxyphenoxy)propane-1,3-diol

Chemical Property:

Purity/Quality:

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Technology Process of (1S, 2R)-1-(4-hydroxy-3-methoxyphenyl)-2-(2-methoxyphenoxy)propane-1,3-diol

There total 10 articles about (1S, 2R)-1-(4-hydroxy-3-methoxyphenyl)-2-(2-methoxyphenoxy)propane-1,3-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

C29H48O6Si2 (1357023-50-7) → (1S, 2R)-1-(4-hydroxy-3-methoxyphenyl)-2-(2-methoxyphenoxy)propane-1,3-diol (1189197-76-9)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

DOI:10.1016/j.tetlet.2011.12.016

Reference yield: 88.8%

C20H24O6 (1357023-47-2) → (1S, 2R)-1-(4-hydroxy-3-methoxyphenyl)-2-(2-methoxyphenoxy)propane-1,3-diol (1189197-76-9)

Guidance literature:

With hydrogenchloride; water; In tetrahydrofuran; at 0 - 20 ℃; for 12h; Inert atmosphere;

DOI:10.1016/j.tetlet.2011.12.016

Reference yield:

(R)-3-((2S,3S)-3-hydroxy-3-(4-hydroxy-3-methoxyphenyl)-2-(2-methoxyphenoxy)propanoyl)-4-phenyloxazolidin-2-one → (1S, 2R)-1-(4-hydroxy-3-methoxyphenyl)-2-(2-methoxyphenoxy)propane-1,3-diol (1189197-76-9)

Guidance literature:

With sodium tetrahydroborate; hydrogen; In tetrahydrofuran; at 0 ℃; for 1h;

DOI:10.1021/acs.orglett.7b00587

upstream raw materials:

C₂₉H₄₈O₆Si₂

C₂₉H₄₆O₆Si₂

(R)-3-hydroxy-1-(4-hydroxy-3-methoxyphenyl)-2-(2-methoxyphenoxy)propan-1-one

C₂₀H₂₄O₆

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