C₂₆H₂₃NO₃

Base Information

Chemical Name:C₂₆H₂₃NO₃
CAS No.:1395060-02-2
Molecular Formula:C₂₆H₂₃NO₃
Molecular Weight:397.474
Hs Code.:

C<sub>26</sub>H<sub>23</sub>NO<sub>3</sub>

Synonyms:C₂₆H₂₃NO₃

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Chemical Property of C₂₆H₂₃NO₃

Chemical Property:

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Technology Process of C₂₆H₂₃NO₃

There total 13 articles about C₂₆H₂₃NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 57772-57-3
5-hydroxy-2-iodo-benzoic acid

: 1395060-02-2
C₂₆H₂₃NO₃

Guidance literature:: Multi-step reaction with 10 steps

1.1: potassium carbonate / acetone / 5 h / Reflux

2.1: sodium hydroxide / water; methanol / 2 h / Reflux

3.1: Vilsmeier reagent / dichloromethane / 0.5 h / 0 - 20 °C

3.2: 12 h / 0 - 20 °C

4.1: sodium hydride / N,N-dimethyl-formamide / 6.5 h / 0 - 20 °C

5.1: palladium diacetate; triphenylphosphine; sodium acetate / N,N-dimethyl-formamide / 8 h / 100 °C / Inert atmosphere

6.1: boron tribromide / dichloromethane / 3 h / 0 °C / Inert atmosphere

7.1: pyridine / dichloromethane / 2 h / 0 - 20 °C

8.1: bis-triphenylphosphine-palladium(II) chloride; potassium acetate / 1,4-dioxane / 3 h / 120 °C / Inert atmosphere

9.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium phosphate / N,N-dimethyl-formamide / 3 h / 120 °C / Inert atmosphere

10.1: sodium hydroxide / water; ethanol / 3 h / 80 °C

With pyridine; bis-triphenylphosphine-palladium(II) chloride; potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; Vilsmeier reagent; potassium acetate; sodium acetate; palladium diacetate; boron tribromide; sodium hydride; potassium carbonate; triphenylphosphine; sodium hydroxide; In 1,4-dioxane; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; 5.1: |Heck Reaction;
DOI:10.1021/jm3002394

Reference yield:

: 1395060-35-1
methyl 2-(4-(5,11-dihydro-2-ethyl-5-methyl-11-methylene-6-oxodibenz[b,e]azepin-8-yl)phenyl)acetate

: 1395060-02-2
C₂₆H₂₃NO₃

Guidance literature:: With sodium hydroxide; In ethanol; water; at 80 ℃; for 3h;
DOI:10.1021/jm3002394

Reference yield:

: 394-31-0
2-amino-5-hydroxybenzoic acid

: 1395060-02-2
C₂₆H₂₃NO₃

Guidance literature:: Multi-step reaction with 11 steps

1.1: sodium nitrite; hydrogenchloride / 0.5 h / 0 °C

1.2: 0.83 h / 0 - 90 °C

2.1: potassium carbonate / acetone / 5 h / Reflux

3.1: sodium hydroxide / water; methanol / 2 h / Reflux

4.1: Vilsmeier reagent / dichloromethane / 0.5 h / 0 - 20 °C

4.2: 12 h / 0 - 20 °C

5.1: sodium hydride / N,N-dimethyl-formamide / 6.5 h / 0 - 20 °C

6.1: palladium diacetate; triphenylphosphine; sodium acetate / N,N-dimethyl-formamide / 8 h / 100 °C / Inert atmosphere

7.1: boron tribromide / dichloromethane / 3 h / 0 °C / Inert atmosphere

8.1: pyridine / dichloromethane / 2 h / 0 - 20 °C

9.1: bis-triphenylphosphine-palladium(II) chloride; potassium acetate / 1,4-dioxane / 3 h / 120 °C / Inert atmosphere

10.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium phosphate / N,N-dimethyl-formamide / 3 h / 120 °C / Inert atmosphere

11.1: sodium hydroxide / water; ethanol / 3 h / 80 °C

With pyridine; hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; Vilsmeier reagent; potassium acetate; sodium acetate; palladium diacetate; boron tribromide; sodium hydride; potassium carbonate; triphenylphosphine; sodium hydroxide; sodium nitrite; In 1,4-dioxane; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; 6.1: |Heck Reaction;
DOI:10.1021/jm3002394