(E)-2-[3-(4-chlorophenyl)-2-propenyl]-1,2,3,4-tetrahydro-6-isoquinolinol

Base Information

• Chemical Name: (E)-2-[3-(4-chlorophenyl)-2-propenyl]-1,2,3,4-tetrahydro-6-isoquinolinol
• CAS No.: 263395-26-2
• Molecular Formula: C₁₈H₁₈ClNO
• Molecular Weight: 299.8

Synonyms:(E)-2-[3-(4-chlorophenyl)-2-propenyl]-1,2,3,4-tetrahydro-6-isoquinolinol

Chemical Property of (E)-2-[3-(4-chlorophenyl)-2-propenyl]-1,2,3,4-tetrahydro-6-isoquinolinol

Chemical Property:

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Technology Process of (E)-2-[3-(4-chlorophenyl)-2-propenyl]-1,2,3,4-tetrahydro-6-isoquinolinol

There total 1 articles about (E)-2-[3-(4-chlorophenyl)-2-propenyl]-1,2,3,4-tetrahydro-6-isoquinolinol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-hydroxy-1,2,3,4-tetrahydroisoquinoline (14446-24-3) + (E)-1-(4-chlorophenyl)-3-chloropropene (103979-29-9) → (E)-2-[3-(4-chlorophenyl)-2-propenyl]-1,2,3,4-tetrahydro-6-isoquinolinol (263395-26-2)

Guidance literature:

With potassium carbonate; In dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

(E)-2-[3-(4-chlorophenyl)-2-propenyl]-1,2,3,4-tetrahydro-6-isoquinolinol (263395-26-2) + 1-[2-(2,4-difluorophenyl)-2,3-epoxypropyl]-1H-1,2,4-triazole (86386-76-7,123632-22-4,141113-42-0,150024-48-9) → alpha-[[[2-[3-(4-chlorophenyl)-2(E)-propenyl]-1,2,3,4-tetrahydro-6-isoquinolinyl]oxy]methyl]-alpha-(2,4-difluorophenyl)-1H-1,2,4-triazol-1-ethanol

Guidance literature:

With 18-crown-6 ether; potassium carbonate; In DMF (N,N-dimethyl-formamide); at 80 ℃; for 2h;

Reference yield:

(E)-2-[3-(4-chlorophenyl)-2-propenyl]-1,2,3,4-tetrahydro-6-isoquinolinol (263395-26-2) + 1-[[2-(2,4-dichlorophenyl)-oxiranyl]methyl]-1H-imidazole (78202-37-6,87049-58-9,87049-60-3) → alpha-[[[2-[3-(4-chlorophenyl)-2(E)-propenyl]-1,2,3,4-tetrahydro-6-isoquinolinyl]oxy]methyl]-alpha-(2,4-dichlorophenyl)-1H-imidazol-1-ethanol

Guidance literature:

With 18-crown-6 ether; potassium carbonate; In DMF (N,N-dimethyl-formamide); at 80 ℃; for 32h;

upstream raw materials:

6-hydroxy-1,2,3,4-tetrahydroisoquinoline

(E)-1-(4-chlorophenyl)-3-chloropropene

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