2-Iodobenzyl bromide

Base Information

Chemical Name:2-Iodobenzyl bromide
CAS No.:40400-13-3
Molecular Formula:C7H6BrI
Molecular Weight:296.933
Hs Code.:2903999090
European Community (EC) Number:628-053-0
DSSTox Substance ID:DTXSID90465568
Nikkaji Number:J31.705E
Wikidata:Q72483453
Mol file:40400-13-3.mol

Synonyms:2-Iodobenzyl bromide;40400-13-3;1-(bromomethyl)-2-iodobenzene;Benzene, 1-(bromomethyl)-2-iodo-;1-Bromomethyl-2-iodobenzene;MFCD00236046;o-iodobenzyl bromide;alpha-Bromo-2-iodotoluene;2-iodobenzylbromide;ortho-Iodo-benzylbromide;alpha-bromo-2-iodo toluene;2-Iodobenzyl bromide, 97%;SCHEMBL560812;GQFITODJWOIYPF-UHFFFAOYSA-;DTXSID90465568;GQFITODJWOIYPF-UHFFFAOYSA-N;CK2021;AKOS015836008;CS-W007400;GS-5918;AC-26200;AM20040420;FT-0612673;I0635;NS00116575;EN300-215102;A923770;a-Bromo-2-iodotoluene;Benzene,1-(bromomethyl)-2-iodo-;InChI=1/C7H6BrI/c8-5-6-3-1-2-4-7(6)9/h1-4H,5H2

Suppliers and Price of 2-Iodobenzyl bromide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-Iodobenzyl bromide
2.5g
$ 75.00

TCI Chemical
2-Iodobenzyl Bromide
5G
$ 62.00

TCI Chemical
2-Iodobenzyl Bromide
1G
$ 21.00

SynQuest Laboratories
2-Iodobenzyl bromide
100 g
$ 440.00

SynQuest Laboratories
2-Iodobenzyl bromide
25 g
$ 160.00

SynQuest Laboratories
2-Iodobenzyl bromide
5 g
$ 80.00

Sigma-Aldrich
2-Iodobenzyl bromide 97%
5g
$ 75.50

Frontier Specialty Chemicals
2-Iodobenzyl bromide 96%
25g
$ 352.00

Frontier Specialty Chemicals
2-Iodobenzyl bromide 96%
5g
$ 88.00

Frontier Specialty Chemicals
2-Iodobenzyl bromide 96%
1g
$ 31.00

Total 66 raw suppliers

Chemical Property of 2-Iodobenzyl bromide

Chemical Property:

Vapor Pressure:0.007mmHg at 25°C
Melting Point:54-60 °C(lit.)
Refractive Index:1.656
Boiling Point:278.794 °C at 760 mmHg
Flash Point:122.41 °C
PSA：0.00000
Density:2.106 g/cm³
LogP:3.18610
Storage Temp.:Refrigerator
Sensitive.:Light Sensitive
Solubility.:soluble in Methanol
XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:1
Exact Mass:295.86976
Heavy Atom Count:9
Complexity:85

Purity/Quality:

99% ^*data from raw suppliers

2-Iodobenzyl bromide ^*data from reagent suppliers

Safty Information:

Pictogram(s): C; N
Hazard Codes:C,N,T
Statements: 22-34-43-51/53-63-42/43-36/37/38
Safety Statements: 26-36/37/39-61-45-23

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)CBr)I

Technology Process of 2-Iodobenzyl bromide

There total 15 articles about 2-Iodobenzyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 5159-41-1
2-iodobenzyl alcohol

: 40400-13-3
2-Iodobenzyl bromide

Guidance literature:: With phosphorus tribromide; In dichloromethane; at 20 ℃; for 16h;
DOI:10.1016/j.tet.2004.10.105

Reference yield: 93.0%

: 18698-96-9
o-iodophenylacetic acid

: 40400-13-3
2-Iodobenzyl bromide

Guidance literature:: With silver triflate-bis(1,10-phenanthroline) complex; dibromoisocyanuric acid; In 1,2-dichloro-ethane; at 20 ℃; for 12h; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.orglett.7b00439