1-(3-methyl-4-nitrobenzyl)-3-(trifluoromethyl)-5-(trifluoromethylthio)-1H-pyrazole

Base Information

Chemical Name:1-(3-methyl-4-nitrobenzyl)-3-(trifluoromethyl)-5-(trifluoromethylthio)-1H-pyrazole
CAS No.:1207089-75-5
Molecular Formula:C₁₃H₉F₆N₃O₂S
Molecular Weight:385.29
Hs Code.:

Synonyms:1-(3-methyl-4-nitrobenzyl)-3-(trifluoromethyl)-5-(trifluoromethylthio)-1H-pyrazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(3-methyl-4-nitrobenzyl)-3-(trifluoromethyl)-5-(trifluoromethylthio)-1H-pyrazole

Chemical Property:

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Technology Process of 1-(3-methyl-4-nitrobenzyl)-3-(trifluoromethyl)-5-(trifluoromethylthio)-1H-pyrazole

There total 3 articles about 1-(3-methyl-4-nitrobenzyl)-3-(trifluoromethyl)-5-(trifluoromethylthio)-1H-pyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2314-97-8,263005-66-9
iodotrifluoromethane

: 1289642-94-9
1-(3-methyl-4-nitrobenzyl)-3-(trifluoromethyl)-1H-pyrazole-5-thiol

: 1207089-75-5
1-(3-methyl-4-nitrobenzyl)-3-(trifluoromethyl)-5-(trifluoromethylthio)-1H-pyrazole

Guidance literature:: With disodium hydrogenphosphate; sodium dithionite; In water; N,N-dimethyl-formamide; at 20 ℃; for 7h; Sealed;

Reference yield:

: 866638-96-2
(3-methyl-4-nitrobenzyl)-hydrazine

: 1207089-75-5
1-(3-methyl-4-nitrobenzyl)-3-(trifluoromethyl)-5-(trifluoromethylthio)-1H-pyrazole

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / toluene / 8 h / Reflux

2: Lawessons reagent / toluene / 12 h / Reflux

3: disodium hydrogenphosphate; sodium dithionite / water; N,N-dimethyl-formamide / 7 h / 20 °C / Sealed

With Lawessons reagent; disodium hydrogenphosphate; sodium dithionite; toluene-4-sulfonic acid; In water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1207089-72-2
1-(3-methyl-4-nitrobenzyl)-3-(trifluoromethyl)-1H-pyrazol-5-ol

: 1207089-75-5
1-(3-methyl-4-nitrobenzyl)-3-(trifluoromethyl)-5-(trifluoromethylthio)-1H-pyrazole

Guidance literature:: Multi-step reaction with 2 steps

1: Lawessons reagent / toluene / 12 h / Reflux

2: disodium hydrogenphosphate; sodium dithionite / water; N,N-dimethyl-formamide / 7 h / 20 °C / Sealed

With Lawessons reagent; disodium hydrogenphosphate; sodium dithionite; In water; N,N-dimethyl-formamide; toluene;