ethyl N-(4-{(1R)-1-[(R)-(4-chlorophenyl)(hydroxy)methyl]butyl}benzoyl)-β-alaninate

Base Information

Chemical Name:ethyl N-(4-{(1R)-1-[(R)-(4-chlorophenyl)(hydroxy)methyl]butyl}benzoyl)-β-alaninate
CAS No.:1232143-68-8
Molecular Formula:C₂₃H₂₈ClNO₄
Molecular Weight:417.933
Hs Code.:

Synonyms:ethyl N-(4-{(1R)-1-[(R)-(4-chlorophenyl)(hydroxy)methyl]butyl}benzoyl)-β-alaninate

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Chemical Property of ethyl N-(4-{(1R)-1-[(R)-(4-chlorophenyl)(hydroxy)methyl]butyl}benzoyl)-β-alaninate

Chemical Property:

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Technology Process of ethyl N-(4-{(1R)-1-[(R)-(4-chlorophenyl)(hydroxy)methyl]butyl}benzoyl)-β-alaninate

There total 1 articles about ethyl N-(4-{(1R)-1-[(R)-(4-chlorophenyl)(hydroxy)methyl]butyl}benzoyl)-β-alaninate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1232143-62-2
4-{(1R)-1-[(R)-(4-chlorophenyl)(hydroxyl)methyl]butyl}benzoic acid

: 4244-84-2
ethyl β-alaninate hydrochloride

: 1232143-68-8
ethyl N-(4-{(1R)-1-[(R)-(4-chlorophenyl)(hydroxy)methyl]butyl}benzoyl)-β-alaninate

Guidance literature:: 4-{(1R)-1-[(R)-(4-chlorophenyl)(hydroxyl)methyl]butyl}benzoic acid; With 1,1'-carbonyldiimidazole; In tetrahydrofuran; at 20 ℃; for 1h;

ethyl β-alaninate hydrochloride; In tetrahydrofuran; at 20 ℃; for 48h;

Reference yield:

: 1232143-68-8
ethyl N-(4-{(1R)-1-[(R)-(4-chlorophenyl)(hydroxy)methyl]butyl}benzoyl)-β-alaninate

: 1027511-98-3
1-bromo-2-chloro-5-fluoro-3-(trifluoromethyl)benzene

: 1242063-05-3
N-(4-{(1R)-1-[(R)-[3-bromo-4-chloro-5-(trifluoromethyl)phenoxy](4-chlorophenyl)methyl]butyl}benzoyl)-β-alanine

Guidance literature:: ethyl N-(4-{(1R)-1-[(R)-(4-chlorophenyl)(hydroxy)methyl]butyl}benzoyl)-β-alaninate; 1-bromo-2-chloro-5-fluoro-3-(trifluoromethyl)benzene; With sodium t-butanolate; In N,N-dimethyl-formamide; at 120 ℃; for 12h;

With hydrogenchloride; water; In ethyl acetate; N,N-dimethyl-formamide; at 20 ℃;