methyl (3-methoxy-2-{3-[3-(1-methylethyl)-1-(5-nitro-2-pyridyl)-1H-pyrazol-4-yl]propoxy}phenyl)acetate

Base Information

Chemical Name:methyl (3-methoxy-2-{3-[3-(1-methylethyl)-1-(5-nitro-2-pyridyl)-1H-pyrazol-4-yl]propoxy}phenyl)acetate
CAS No.:628331-38-4
Molecular Formula:C₂₄H₂₈N₄O₆
Molecular Weight:468.51
Hs Code.:

Synonyms:methyl (3-methoxy-2-{3-[3-(1-methylethyl)-1-(5-nitro-2-pyridyl)-1H-pyrazol-4-yl]propoxy}phenyl)acetate

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Chemical Property of methyl (3-methoxy-2-{3-[3-(1-methylethyl)-1-(5-nitro-2-pyridyl)-1H-pyrazol-4-yl]propoxy}phenyl)acetate

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Technology Process of methyl (3-methoxy-2-{3-[3-(1-methylethyl)-1-(5-nitro-2-pyridyl)-1H-pyrazol-4-yl]propoxy}phenyl)acetate

There total 11 articles about methyl (3-methoxy-2-{3-[3-(1-methylethyl)-1-(5-nitro-2-pyridyl)-1H-pyrazol-4-yl]propoxy}phenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 3-[3-(1-methylethyl)-1-(5-nitro-2-pyridyl)-1H-pyrazol-4-yl]-1-propanol

: 103324-26-1
(2-hydroxy-3-methoxyphenyl)acetic acid methyl ester

: 628331-38-4
methyl (3-methoxy-2-{3-[3-(1-methylethyl)-1-(5-nitro-2-pyridyl)-1H-pyrazol-4-yl]propoxy}phenyl)acetate

Guidance literature:: With tributylphosphine; 1,1'-azodicarbonyl-dipiperidine; at 20 ℃;

Reference yield:

: 628331-26-0
[1-benzyl-3-(1-methylethyl)-1H-pyrazol-4-yl]methanol

: 628331-38-4
methyl (3-methoxy-2-{3-[3-(1-methylethyl)-1-(5-nitro-2-pyridyl)-1H-pyrazol-4-yl]propoxy}phenyl)acetate

Guidance literature:: Multi-step reaction with 7 steps

1.1: manganese(IV) oxide / tetrahydrofuran / 20 °C

1.2: 0 - 20 °C

2.1: hydrogen / 5%-palladium/activated carbon / tetrahydrofuran / 20 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 - 20 °C

4.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 - 20 °C

5.1: hydrogen / 5%-palladium/activated carbon / tetrahydrofuran / 50 °C

6.1: sodium hydride / DMF (N,N-dimethyl-formamide) / 3 h / 0 - 80 °C

6.2: 60 °C

7.1: tributylphosphine; 1,1'-azodicarbonyl-dipiperidine / 20 °C

With manganese(IV) oxide; lithium aluminium tetrahydride; tributylphosphine; hydrogen; sodium hydride; N-ethyl-N,N-diisopropylamine; 1,1'-azodicarbonyl-dipiperidine; 5%-palladium/activated carbon; In tetrahydrofuran; DMF (N,N-dimethyl-formamide);

Reference yield:

: 628331-25-9
methyl 1-benzyl-3-(1-methylethyl)-1H-pyrazole-4-carboxylate

: 628331-38-4
methyl (3-methoxy-2-{3-[3-(1-methylethyl)-1-(5-nitro-2-pyridyl)-1H-pyrazol-4-yl]propoxy}phenyl)acetate

Guidance literature:: Multi-step reaction with 8 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 - 20 °C

2.1: manganese(IV) oxide / tetrahydrofuran / 20 °C

2.2: 0 - 20 °C

3.1: hydrogen / 5%-palladium/activated carbon / tetrahydrofuran / 20 °C

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 - 20 °C

5.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 - 20 °C

6.1: hydrogen / 5%-palladium/activated carbon / tetrahydrofuran / 50 °C

7.1: sodium hydride / DMF (N,N-dimethyl-formamide) / 3 h / 0 - 80 °C

7.2: 60 °C

8.1: tributylphosphine; 1,1'-azodicarbonyl-dipiperidine / 20 °C

With manganese(IV) oxide; lithium aluminium tetrahydride; tributylphosphine; hydrogen; sodium hydride; N-ethyl-N,N-diisopropylamine; 1,1'-azodicarbonyl-dipiperidine; 5%-palladium/activated carbon; In tetrahydrofuran; DMF (N,N-dimethyl-formamide);