N,N-dibenzyl-6-azido-1-O-benzyl-6-deoxy-2,3-O-isopropylidene-D-glycero-α-D-manno-heptofuranuronamide

Base Information

• Chemical Name: N,N-dibenzyl-6-azido-1-O-benzyl-6-deoxy-2,3-O-isopropylidene-D-glycero-α-D-manno-heptofuranuronamide
• CAS No.: 1017834-05-7
• Molecular Formula: C₃₁H₃₄N₄O₆
• Molecular Weight: 558.634

Synonyms:N,N-dibenzyl-6-azido-1-O-benzyl-6-deoxy-2,3-O-isopropylidene-D-glycero-α-D-manno-heptofuranuronamide

Chemical Property of N,N-dibenzyl-6-azido-1-O-benzyl-6-deoxy-2,3-O-isopropylidene-D-glycero-α-D-manno-heptofuranuronamide

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Technology Process of N,N-dibenzyl-6-azido-1-O-benzyl-6-deoxy-2,3-O-isopropylidene-D-glycero-α-D-manno-heptofuranuronamide

There total 1 articles about N,N-dibenzyl-6-azido-1-O-benzyl-6-deoxy-2,3-O-isopropylidene-D-glycero-α-D-manno-heptofuranuronamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

C31H33NO6 (1017834-03-5) → N,N-dibenzyl-6-azido-1-O-benzyl-6-deoxy-2,3-O-isopropylidene-D-glycero-α-D-manno-heptofuranuronamide (1017834-05-7)

Guidance literature:

With sodium azide; acetic acid; In N,N-dimethyl-formamide; at 95 ℃; for 48h; regioselective reaction; Inert atmosphere;

DOI:10.1016/j.tetasy.2010.06.035

Reference yield: 69.0%

N,N-dibenzyl-6-azido-1-O-benzyl-6-deoxy-2,3-O-isopropylidene-D-glycero-α-D-manno-heptofuranuronamide (1017834-05-7) → C24H30N2O5 (1017834-11-5)

Guidance literature:

With palladium 10% on activated carbon; ammonium formate; In methanol; for 48h; Reflux;

DOI:10.1016/j.tetasy.2010.06.035

upstream raw materials:

C₃₁H₃₃NO₆

Downstream raw materials:

C₂₄H₃₀N₂O₅

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