C₆₂H₄₈BN₃O₃S₂

Base Information

Chemical Name:C₆₂H₄₈BN₃O₃S₂
CAS No.:1308305-26-1
Molecular Formula:C₆₂H₄₈BN₃O₃S₂
Molecular Weight:958.024
Hs Code.:

C<sub>62</sub>H<sub>48</sub>BN<sub>3</sub>O<sub>3</sub>S<sub>2</sub>

Synonyms:C₆₂H₄₈BN₃O₃S₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₂H₄₈BN₃O₃S₂

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Technology Process of C₆₂H₄₈BN₃O₃S₂

There total 11 articles about C₆₂H₄₈BN₃O₃S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: GF

: 1173167-31-1
C₁₃H₁₃NO

: 34993-56-1
1-ethynylpyrene

: 1308305-26-1
C₆₂H₄₈BN₃O₃S₂

Guidance literature:: C₁₃H₁₃NO; 1-ethynylpyrene; With ethylmagnesium bromide; In tetrahydrofuran; at 50 ℃; for 2h; Inert atmosphere;

GF; In tetrahydrofuran; at 25 - 70 ℃; for 16h; Inert atmosphere;
DOI:10.1021/jo200246q

Reference yield:

: 872-55-9
2-ethylthiophene

: 1308305-26-1
C₆₂H₄₈BN₃O₃S₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: n-butyllithium / tetrahydrofuran; hexanes / 1 h / -78 °C / Inert atmosphere

1.2: 1 h / -78 °C / Inert atmosphere

2.1: hydrazine hydrate / ethanol / 12 h / Reflux; Inert atmosphere

3.1: 1 h / 75 °C / Inert atmosphere

4.1: lead(IV) tetraacetate / tetrahydrofuran / 1 h / 25 °C / Inert atmosphere

5.1: ammonium acetate; ammonium chloride / ethanol; acetic acid / 0.5 h / 90 °C / Inert atmosphere

6.1: boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Inert atmosphere

7.1: ethylmagnesium bromide / tetrahydrofuran / 2 h / 50 °C / Inert atmosphere

7.2: 16 h / 25 - 70 °C / Inert atmosphere

With n-butyllithium; boron trifluoride diethyl etherate; ethylmagnesium bromide; ammonium acetate; lead(IV) tetraacetate; ammonium chloride; hydrazine hydrate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; hexanes; ethanol; dichloromethane; acetic acid;
DOI:10.1021/jo200246q

Reference yield:

: (E)-5-ethyl-N'-(1-(2-hydroxy-4-methoxyphenyl)ethylidene)-thiophene-2-carbohydrazide

: 1308305-26-1
C₆₂H₄₈BN₃O₃S₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: lead(IV) tetraacetate / tetrahydrofuran / 1 h / 25 °C / Inert atmosphere

2.1: ammonium acetate; ammonium chloride / ethanol; acetic acid / 0.5 h / 90 °C / Inert atmosphere

3.1: boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Inert atmosphere

4.1: ethylmagnesium bromide / tetrahydrofuran / 2 h / 50 °C / Inert atmosphere

4.2: 16 h / 25 - 70 °C / Inert atmosphere

With boron trifluoride diethyl etherate; ethylmagnesium bromide; ammonium acetate; lead(IV) tetraacetate; ammonium chloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; dichloromethane; acetic acid;
DOI:10.1021/jo200246q