1,2,3,4-Tetrahydro-6,7-dimethoxy-4-(3-methoxyphenyl)-3,3-dimethylisoquinoline Hydrochloride

Base Information

Chemical Name:1,2,3,4-Tetrahydro-6,7-dimethoxy-4-(3-methoxyphenyl)-3,3-dimethylisoquinoline Hydrochloride
CAS No.:82416-58-8
Molecular Formula:C₂₀H₂₅NO₃*ClH
Molecular Weight:363.884
Hs Code.:

Synonyms:1,2,3,4-Tetrahydro-6,7-dimethoxy-4-(3-methoxyphenyl)-3,3-dimethylisoquinoline Hydrochloride

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Chemical Property of 1,2,3,4-Tetrahydro-6,7-dimethoxy-4-(3-methoxyphenyl)-3,3-dimethylisoquinoline Hydrochloride

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Technology Process of 1,2,3,4-Tetrahydro-6,7-dimethoxy-4-(3-methoxyphenyl)-3,3-dimethylisoquinoline Hydrochloride

There total 4 articles about 1,2,3,4-Tetrahydro-6,7-dimethoxy-4-(3-methoxyphenyl)-3,3-dimethylisoquinoline Hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 82416-48-6
α-<1-<<(3,4-dimethoxyphenyl)methyl>amino>-1-methylethyl>-3-methoxybenzenemethanol

: 82416-58-8
1,2,3,4-Tetrahydro-6,7-dimethoxy-4-(3-methoxyphenyl)-3,3-dimethylisoquinoline Hydrochloride

Guidance literature:: With PPA; at 80 ℃; for 4h;
DOI:10.1002/jhet.5570190102

Reference yield:

: 73866-99-6
α-(1-amino-1-methylethyl)-3-methoxybenzenemethanol

: 82416-58-8
1,2,3,4-Tetrahydro-6,7-dimethoxy-4-(3-methoxyphenyl)-3,3-dimethylisoquinoline Hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

2: KBH₄ / methanol

3: 76 percent / polyphosphoric acid / 4 h / 80 °C

With PPA; potassium borohydride; In methanol;
DOI:10.1002/jhet.5570190102

Reference yield:

: 2-{[1-(3,4-Dimethoxy-phenyl)-meth-(Z)-ylidene]-amino}-1-(3-methoxy-phenyl)-2-methyl-propan-1-ol

: 82416-58-8
1,2,3,4-Tetrahydro-6,7-dimethoxy-4-(3-methoxyphenyl)-3,3-dimethylisoquinoline Hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: KBH₄ / methanol

2: 76 percent / polyphosphoric acid / 4 h / 80 °C

With PPA; potassium borohydride; In methanol;
DOI:10.1002/jhet.5570190102