3-<2-amino>ethyl>-N-<(trifluoromethyl)sulfonyl>indoline

Base Information

Chemical Name:3-<2-amino>ethyl>-N-<(trifluoromethyl)sulfonyl>indoline
CAS No.:169129-69-5
Molecular Formula:C₁₉H₁₉F₃N₂O₄S
Molecular Weight:428.432
Hs Code.:

3-<2-<N-<(benzyloxy)carbonyl>amino>ethyl>-N-<(trifluoromethyl)sulfonyl>indoline

Synonyms:3-<2-amino>ethyl>-N-<(trifluoromethyl)sulfonyl>indoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-<2-amino>ethyl>-N-<(trifluoromethyl)sulfonyl>indoline

Chemical Property:

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Technology Process of 3-<2-amino>ethyl>-N-<(trifluoromethyl)sulfonyl>indoline

There total 4 articles about 3-<2-amino>ethyl>-N-<(trifluoromethyl)sulfonyl>indoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 169129-68-4
3-<2-amino>ethyl>indoline

: 169129-69-5
3-<2-amino>ethyl>-N-<(trifluoromethyl)sulfonyl>indoline

Guidance literature:: With triethylamine; In dichloromethane; at -78 ℃; for 0.5h;
DOI:10.1021/ja00141a004

Reference yield:

: 61-54-1
tryptamine

: 169129-69-5
3-<2-amino>ethyl>-N-<(trifluoromethyl)sulfonyl>indoline

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / NaOH / tetrahydrofuran

2: 97 percent / BH₃*THF, TFA / tetrahydrofuran / 0.5 h / 0 °C

3: 88 percent / Et₃N / CH₂Cl₂ / 0.5 h / -78 °C

With sodium hydroxide; borane-THF; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00141a004

Reference yield:

: 38750-13-9
(2-indol-3-yl-ethyl)-carbamic acid benzyl ester

: 169129-69-5
3-<2-amino>ethyl>-N-<(trifluoromethyl)sulfonyl>indoline

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / BH₃*THF, TFA / tetrahydrofuran / 0.5 h / 0 °C

2: 88 percent / Et₃N / CH₂Cl₂ / 0.5 h / -78 °C

With borane-THF; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00141a004