1,3-diphenylprop-1-yl phenyl sulfide

Base Information

• Chemical Name: 1,3-diphenylprop-1-yl phenyl sulfide
• CAS No.: 69333-51-3
• Molecular Formula: C₂₁H₂₀S
• Molecular Weight: 304.456
• Mol file: 69333-51-3.mol

Synonyms:1,3-diphenylprop-1-yl phenyl sulfide

Chemical Property of 1,3-diphenylprop-1-yl phenyl sulfide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,3-diphenylprop-1-yl phenyl sulfide

There total 2 articles about 1,3-diphenylprop-1-yl phenyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + Benzyl phenyl sulfide (831-91-4) → 1,3-diphenylprop-1-yl phenyl sulfide (69333-51-3)

Guidance literature:

With potassium hexamethylsilazane; In diethyl ether; at 40 ℃; for 24h; Solvent; Temperature; Time; chemoselective reaction; Catalytic behavior; Sealed tube; Schlenk technique; Inert atmosphere;

DOI:10.1021/acs.orglett.9b01994

Reference yield: 82.0%

1,3-diphenylprop-2-yl 2-[2-(4-methoxyphenyl)ethynyl]benzoate + thiophenol (108-98-5) → 1,3-diphenylprop-1-yl phenyl sulfide (69333-51-3) + 3-(4-methoxyphenyl)-1H-isochromen-1-one (29910-92-7)

Guidance literature:

With (triphenylphosphine)gold(I) chloride; silver trifluoromethanesulfonate; In 1,2-dichloro-ethane; at 80 ℃; for 15h; Inert atmosphere; Darkness;

DOI:10.1016/j.tetlet.2009.11.025

Reference yield: 87.0%

1,3-diphenylprop-1-yl phenyl sulfide (69333-51-3) → 1,3-diphenylpropane (1081-75-0)

Guidance literature:

With triethylsilane; tris(pentafluorophenyl)borate; In chloroform-d1; for 2h;

DOI:10.1021/acs.orglett.9b01994

upstream raw materials:

thiophenol

styrene

Benzyl phenyl sulfide

Downstream raw materials:

1,3-diphenylpropane