C₁₈H₂₃NO₃

Base Information

Chemical Name:C₁₈H₂₃NO₃
CAS No.:1416815-16-1
Molecular Formula:C₁₈H₂₃NO₃
Molecular Weight:301.386
Hs Code.:

C<sub>18</sub>H<sub>23</sub>NO<sub>3</sub>

Synonyms:C₁₈H₂₃NO₃

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Chemical Property of C₁₈H₂₃NO₃

Chemical Property:

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Technology Process of C₁₈H₂₃NO₃

There total 6 articles about C₁₈H₂₃NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1416815-31-0
(6S,11S)-11-(benzyloxymethyl)-2-azaspiro[5.5]undec-8-ene-1,7-dione

: 1416815-16-1
C₁₈H₂₃NO₃

Guidance literature:: (6S,11S)-11-(benzyloxymethyl)-2-azaspiro[5.5]undec-8-ene-1,7-dione; With cerium(III) chloride heptahydrate; In methanol; at 20 ℃; for 0.166667h; Inert atmosphere;

With sodium tetrahydroborate; In methanol; at -78 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ol3030764

Reference yield:

: 954148-38-0
methyl (1R,6S)-6-(benzyloxymethyl)cyclohex-3-enecarboxylate

: 1416815-16-1
C₁₈H₂₃NO₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 2 h / -78 °C / Inert atmosphere

1.2: 18 h / -78 - 20 °C / Inert atmosphere

2.1: triphenylphosphine; water / tetrahydrofuran / 2 h / Reflux; Inert atmosphere

3.1: potassium carbonate / methanol; water / 18 h / 20 °C / Inert atmosphere

4.1: selenium(IV) oxide; water / ethanol / 72 h / 90 °C / Inert atmosphere

5.1: manganese(IV) oxide / toluene / 18 h / Molecular sieve; Reflux; Inert atmosphere

6.1: cerium(III) chloride heptahydrate / methanol / 0.17 h / 20 °C / Inert atmosphere

6.2: 0.5 h / -78 °C / Inert atmosphere

With manganese(IV) oxide; selenium(IV) oxide; cerium(III) chloride heptahydrate; water; potassium hexamethylsilazane; potassium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; ethanol; water; toluene; 2.1: |Staudinger Azide Reduction / 6.2: |Luche Cerium Reduction;
DOI:10.1021/ol3030764

Reference yield:

: 1416815-14-9
(6R,11S)-11-(benzyloxymethyl)-2-azaspiro[5.5]undec-8-en-1-one

: 1416815-16-1
C₁₈H₂₃NO₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: selenium(IV) oxide; water / ethanol / 72 h / 90 °C / Inert atmosphere

2.1: manganese(IV) oxide / toluene / 18 h / Molecular sieve; Reflux; Inert atmosphere

3.1: cerium(III) chloride heptahydrate / methanol / 0.17 h / 20 °C / Inert atmosphere

3.2: 0.5 h / -78 °C / Inert atmosphere

With manganese(IV) oxide; selenium(IV) oxide; cerium(III) chloride heptahydrate; water; In methanol; ethanol; toluene; 3.2: |Luche Cerium Reduction;
DOI:10.1021/ol3030764