(RuH(NH₂CH₂CH₃)2(CH₃C(CH₂As(C₆H₅)2)3))⁽¹⁺⁾*CF₃SO₃^(1-)=(RuH(NH₂CH₂CH₃)2(CH₃C(CH₂As(C₆H₅)2)3))CF₃SO₃

Base Information

• Chemical Name: (RuH(NH₂CH₂CH₃)2(CH₃C(CH₂As(C₆H₅)2)3))⁽¹⁺⁾*CF₃SO₃^(1-)=(RuH(NH₂CH₂CH₃)2(CH₃C(CH₂As(C₆H₅)2)3))CF₃SO₃
• CAS No.: 109124-80-3
• Molecular Formula: CF₃O₃S*C₄₅H₅₄As₃N₂Ru
• Molecular Weight: 1097.84

Synonyms:(RuH(NH₂CH₂CH₃)2(CH₃C(CH₂As(C₆H₅)2)3))⁽¹⁺⁾*CF₃SO₃^(1-)=(RuH(NH₂CH₂CH₃)2(CH₃C(CH₂As(C₆H₅)2)3))CF₃SO₃

Chemical Property of (RuH(NH₂CH₂CH₃)2(CH₃C(CH₂As(C₆H₅)2)3))⁽¹⁺⁾*CF₃SO₃^(1-)=(RuH(NH₂CH₂CH₃)2(CH₃C(CH₂As(C₆H₅)2)3))CF₃SO₃

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Technology Process of (RuH(NH₂CH₂CH₃)2(CH₃C(CH₂As(C₆H₅)2)3))⁽¹⁺⁾*CF₃SO₃^(1-)=(RuH(NH₂CH₂CH₃)2(CH₃C(CH₂As(C₆H₅)2)3))CF₃SO₃

There total 1 articles about (RuH(NH₂CH₂CH₃)2(CH₃C(CH₂As(C₆H₅)2)3))⁽¹⁺⁾*CF₃SO₃^(1-)=(RuH(NH₂CH₂CH₃)2(CH₃C(CH₂As(C₆H₅)2)3))CF₃SO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

sodium tetrahydroborate (16940-66-2) + Ru(CH3CN)3(CH3C(CH2As(C6H5)2)3)(2+)*2CF3SO3(1-)={Ru(CH3CN)3(CH3C(CH2As(C6H5)2)3)}(CF3SO3)2 (109124-78-9) → (RuH(NH2CH2CH3)2(CH3C(CH2As(C6H5)2)3))(1+)*CF3SO3(1-)=(RuH(NH2CH2CH3)2(CH3C(CH2As(C6H5)2)3))CF3SO3 (109124-80-3)

Guidance literature:

With methanol; In methanol; byproducts: ethylamine; solid NaBH4 (2.0 mmol) was added slowly to a stirred MeOH soln. of Ru-compd. (0.20 mmol); the small amt.of ppt. formed was filtered off;; a MeOH/H2O mixt. (1:1 v/v) was added to the filtrate with formation of an off-white solid; this was filtered out, washed (H2O, MeOH, Et2O) and dried; elem. anal.;;

upstream raw materials:

sodium tetrahydroborate

Ru(CH₃CN)3(CH₃C(CH₂As(C₆H₅)2)3)⁽²⁺⁾*2CF₃SO₃^(1-)={Ru(CH₃CN)3(CH₃C(CH₂As(C₆H₅)2)3)}(CF₃SO₃)2

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