(Amino-p-tolyl-methyl)-phenyl-phosphinic acid phenyl ester; hydrobromide

Base Information

Chemical Name:(Amino-p-tolyl-methyl)-phenyl-phosphinic acid phenyl ester; hydrobromide
CAS No.:110814-63-6
Molecular Formula:BrH*C₂₀H₂₀NO₂P
Molecular Weight:418.27
Hs Code.:

Synonyms:(Amino-p-tolyl-methyl)-phenyl-phosphinic acid phenyl ester; hydrobromide

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Chemical Property of (Amino-p-tolyl-methyl)-phenyl-phosphinic acid phenyl ester; hydrobromide

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Technology Process of (Amino-p-tolyl-methyl)-phenyl-phosphinic acid phenyl ester; hydrobromide

There total 3 articles about (Amino-p-tolyl-methyl)-phenyl-phosphinic acid phenyl ester; hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 110814-57-8
[(Ethoxy-phenoxy-thiophosphorylamino)-p-tolyl-methyl]-phenyl-phosphinic acid phenyl ester

: 110814-63-6
(Amino-p-tolyl-methyl)-phenyl-phosphinic acid phenyl ester; hydrobromide

Guidance literature:: With hydrogen bromide; In acetic acid; for 0.5h; Ambient temperature;
DOI:10.1055/s-1986-31790

Reference yield:

: 13410-61-2
diphenyl phenylphosphonite

: 110814-63-6
(Amino-p-tolyl-methyl)-phenyl-phosphinic acid phenyl ester; hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) BF₃*Et₂O / 1.) DME, room temp., 20 min; 80 deg C, 15 min, 2.) reflux, 5 h

2: 84 percent / HBr / acetic acid / 0.5 h / Ambient temperature

With boron trifluoride diethyl etherate; hydrogen bromide; In acetic acid;
DOI:10.1055/s-1986-31790

Reference yield:

: 104-87-0
4-methyl-benzaldehyde

: 110814-63-6
(Amino-p-tolyl-methyl)-phenyl-phosphinic acid phenyl ester; hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) BF₃*Et₂O / 1.) DME, room temp., 20 min; 80 deg C, 15 min, 2.) reflux, 5 h

2: 84 percent / HBr / acetic acid / 0.5 h / Ambient temperature

With boron trifluoride diethyl etherate; hydrogen bromide; In acetic acid;
DOI:10.1055/s-1986-31790