1,2-dibromo-2-methyl-7-phenoxyheptane

Base Information

Chemical Name:1,2-dibromo-2-methyl-7-phenoxyheptane
CAS No.:257290-45-2
Molecular Formula:C₁₄H₂₀Br₂O
Molecular Weight:364.12
Hs Code.:

Synonyms:1,2-dibromo-2-methyl-7-phenoxyheptane

Suppliers and Price of 1,2-dibromo-2-methyl-7-phenoxyheptane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-dibromo-2-methyl-7-phenoxyheptane

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Technology Process of 1,2-dibromo-2-methyl-7-phenoxyheptane

There total 2 articles about 1,2-dibromo-2-methyl-7-phenoxyheptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 257290-42-9
2-methyl-7-phenoxyhept-1-ene

: 257290-45-2
1,2-dibromo-2-methyl-7-phenoxyheptane

Guidance literature:: With bromine; In diethyl ether; at -50 ℃; for 0.5h;
DOI:10.1021/jo991311z

Reference yield:

: 1200-03-9
4-bromophenyl butyl ether

: 257290-45-2
1,2-dibromo-2-methyl-7-phenoxyheptane

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / CuI / diethyl ether; tetrahydrofuran / 2 h / 20 °C

2: 93 percent / Br₂ / diethyl ether / 0.5 h / -50 °C

With copper(l) iodide; bromine; In tetrahydrofuran; diethyl ether; 1: Grignard reaction / 2: Bromination;
DOI:10.1021/jo991311z