3,4-dichlorophenyl tert-butyl(2,3-dichloro-6-vinyloxyphenyl)phosphinate

Base Information

Chemical Name:3,4-dichlorophenyl tert-butyl(2,3-dichloro-6-vinyloxyphenyl)phosphinate
CAS No.:1224895-40-2
Molecular Formula:C₁₈H₁₇Cl₄O₃P
Molecular Weight:454.117
Hs Code.:

Synonyms:3,4-dichlorophenyl tert-butyl(2,3-dichloro-6-vinyloxyphenyl)phosphinate

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Chemical Property of 3,4-dichlorophenyl tert-butyl(2,3-dichloro-6-vinyloxyphenyl)phosphinate

Chemical Property:

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Technology Process of 3,4-dichlorophenyl tert-butyl(2,3-dichloro-6-vinyloxyphenyl)phosphinate

There total 3 articles about 3,4-dichlorophenyl tert-butyl(2,3-dichloro-6-vinyloxyphenyl)phosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1224895-85-5
3,4-dichlorophenyl tert-butyl(2,3-dichloro-6-hydroxyphenyl)phosphinate

: 1112-56-7
tetravinyltin (IV)

: 1224895-40-2
3,4-dichlorophenyl tert-butyl(2,3-dichloro-6-vinyloxyphenyl)phosphinate

Guidance literature:: With oxygen; copper diacetate; In acetonitrile; at 20 ℃; for 20h;
DOI:10.1002/adsc.200900304

Reference yield:

: 95-77-2
3,4-dichlorophenol

: 1224895-40-2
3,4-dichlorophenyl tert-butyl(2,3-dichloro-6-vinyloxyphenyl)phosphinate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / tetrahydrofuran / 1 h / 0 °C

2: n-butyllithium / tetrahydrofuran / -78 - 20 °C

3: oxygen; copper diacetate / acetonitrile / 20 h / 20 °C

With n-butyllithium; oxygen; copper diacetate; sodium hydride; In tetrahydrofuran; acetonitrile;
DOI:10.1002/adsc.200900304

Reference yield:

: 1224895-75-3
tert-butylphosphonic acid di(3,4-dichlorophenyl) ester

: 1224895-40-2
3,4-dichlorophenyl tert-butyl(2,3-dichloro-6-vinyloxyphenyl)phosphinate

Guidance literature:: Multi-step reaction with 2 steps

1: n-butyllithium / tetrahydrofuran / -78 - 20 °C

2: oxygen; copper diacetate / acetonitrile / 20 h / 20 °C

With n-butyllithium; oxygen; copper diacetate; In tetrahydrofuran; acetonitrile;
DOI:10.1002/adsc.200900304