(2R,3S)-1-tert-butyldimethylsilyloxy-3-tert-butoxycarbonylamino-2-phenylcarbonyloxybutane

Base Information

Chemical Name:(2R,3S)-1-tert-butyldimethylsilyloxy-3-tert-butoxycarbonylamino-2-phenylcarbonyloxybutane
CAS No.:174282-88-3
Molecular Formula:C₂₂H₃₇NO₅Si
Molecular Weight:423.625
Hs Code.:

Synonyms:(2R,3S)-1-tert-butyldimethylsilyloxy-3-tert-butoxycarbonylamino-2-phenylcarbonyloxybutane

Suppliers and Price of (2R,3S)-1-tert-butyldimethylsilyloxy-3-tert-butoxycarbonylamino-2-phenylcarbonyloxybutane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3S)-1-tert-butyldimethylsilyloxy-3-tert-butoxycarbonylamino-2-phenylcarbonyloxybutane

Chemical Property:

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Technology Process of (2R,3S)-1-tert-butyldimethylsilyloxy-3-tert-butoxycarbonylamino-2-phenylcarbonyloxybutane

There total 3 articles about (2R,3S)-1-tert-butyldimethylsilyloxy-3-tert-butoxycarbonylamino-2-phenylcarbonyloxybutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 174282-88-3
(2R,3S)-1-tert-butyldimethylsilyloxy-3-tert-butoxycarbonylamino-2-phenylcarbonyloxybutane

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / H₂ / 20percent Pd(OH)2/C / ethyl acetate / 760 Torr

2: 89 percent / imidazole / dimethylformamide / 6 h / Ambient temperature

3: 80 percent Turnov_. / PPh₃, DEAD / benzene / 12 h

With 1H-imidazole; hydrogen; triphenylphosphine; diethylazodicarboxylate; palladium dihydroxide; In ethyl acetate; N,N-dimethyl-formamide; benzene;
DOI:10.1016/0957-4166(95)00442-4

Reference yield:

: 154079-54-6,174290-53-0,215171-11-2,203933-47-5
(2S,3S)-3-tert-butoxycarbonylamino-1,2-butanediol

: 174282-88-3
(2R,3S)-1-tert-butyldimethylsilyloxy-3-tert-butoxycarbonylamino-2-phenylcarbonyloxybutane

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / imidazole / dimethylformamide / 6 h / Ambient temperature

2: 80 percent Turnov_. / PPh₃, DEAD / benzene / 12 h

With 1H-imidazole; triphenylphosphine; diethylazodicarboxylate; In N,N-dimethyl-formamide; benzene;
DOI:10.1016/0957-4166(95)00442-4