C₂₈H₂₂F₆N₂O₈S

Base Information

Chemical Name:C₂₈H₂₂F₆N₂O₈S
CAS No.:722499-80-1
Molecular Formula:C₂₈H₂₂F₆N₂O₈S
Molecular Weight:660.548
Hs Code.:

C<sub>28</sub>H<sub>22</sub>F<sub>6</sub>N<sub>2</sub>O<sub>8</sub>S

Synonyms:C₂₈H₂₂F₆N₂O₈S

Suppliers and Price of C₂₈H₂₂F₆N₂O₈S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₈H₂₂F₆N₂O₈S

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of C₂₈H₂₂F₆N₂O₈S

There total 12 articles about C₂₈H₂₂F₆N₂O₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 722499-74-3
C₂₇H₂₃F₃N₂O₆

: 722499-80-1
C₂₈H₂₂F₆N₂O₈S

Guidance literature:: With pyridine; at 0 ℃; for 3h;
DOI:10.1002/anie.200353636 DOI:10.1248/cpb.54.1662

Reference yield:

: 722499-78-7
2-(R)-tert-butoxycarbonylamino-N-[2-(4-hydroxyphenyl)ethyl]-3-phenylpropionamide

: 722499-80-1
C₂₈H₂₂F₆N₂O₈S

Guidance literature:: Multi-step reaction with 6 steps

1.1: 97 percent / methanesulfonic acid / methanol / 3 h / 40 °C

2.1: dioxane / 24 h / 20 °C

2.2: 64 percent / HCl / dioxane / 24 h / 20 °C

3.1: 94 percent / pyridine / 0.25 h / 0 °C

4.1: 61 percent / phenyliodine(III) bis(trifluoroacetate) / 2,2,2-trifluoro-ethanol / 0.17 h / -40 °C

5.1: 95 percent / BCl₃ / CH₂Cl₂ / 20 h / -78 °C

6.1: 83 percent / pyridine / 3 h / 0 °C

With pyridine; methanesulfonic acid; boron trichloride; bis-[(trifluoroacetoxy)iodo]benzene; In 1,4-dioxane; methanol; dichloromethane; 2,2,2-trifluoroethanol; 5.1: Michael addition;
DOI:10.1248/cpb.54.1662

Reference yield:

: 722499-70-9
2-(R)-amino-N-[2-(4-hydroxyphenyl)ethyl]-3-phenylpropionamide

: 722499-80-1
C₂₈H₂₂F₆N₂O₈S

Guidance literature:: Multi-step reaction with 5 steps

1.1: dioxane / 24 h / 20 °C

1.2: 64 percent / HCl / dioxane / 24 h / 20 °C

2.1: 94 percent / pyridine / 0.25 h / 0 °C

3.1: 61 percent / phenyliodine(III) bis(trifluoroacetate) / 2,2,2-trifluoro-ethanol / 0.17 h / -40 °C

4.1: 95 percent / BCl₃ / CH₂Cl₂ / 20 h / -78 °C

5.1: 83 percent / pyridine / 3 h / 0 °C

With pyridine; boron trichloride; bis-[(trifluoroacetoxy)iodo]benzene; In 1,4-dioxane; dichloromethane; 2,2,2-trifluoroethanol; 4.1: Michael addition;
DOI:10.1248/cpb.54.1662