C₁₆H₁₀Br₂N₂O₂S

Base Information

Chemical Name:C₁₆H₁₀Br₂N₂O₂S
CAS No.:1312610-44-8
Molecular Formula:C₁₆H₁₀Br₂N₂O₂S
Molecular Weight:454.142
Hs Code.:

C<sub>16</sub>H<sub>10</sub>Br<sub>2</sub>N<sub>2</sub>O<sub>2</sub>S

Synonyms:C₁₆H₁₀Br₂N₂O₂S

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Chemical Property of C₁₆H₁₀Br₂N₂O₂S

Chemical Property:

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Technology Process of C₁₆H₁₀Br₂N₂O₂S

There total 8 articles about C₁₆H₁₀Br₂N₂O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: C₁₄H₆Cl₂N₂O₂S

: 1312610-44-8
C₁₆H₁₀Br₂N₂O₂S

Guidance literature:: diazomethane; C₁₄H₆Cl₂N₂O₂S; In diethyl ether; dichloromethane; at -10 - 0 ℃; for 1h;

With hydrogen bromide; In diethyl ether; dichloromethane; water; at -10 ℃; for 1h;

With sodium hydrogencarbonate; In diethyl ether; dichloromethane; water;

Reference yield:

: 95-54-5
1,2-diamino-benzene

: 1312610-44-8
C₁₆H₁₀Br₂N₂O₂S

Guidance literature:: Multi-step reaction with 7 steps

1.1: thionyl chloride; triethylamine / dichloromethane / 5 h / Reflux

2.1: bromine; hydrogen bromide / water / 4 h / Reflux

3.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water / 12 h / 90 °C / Inert atmosphere

4.1: triethylamine / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 16 h / 120 °C / 15001.5 Torr / Autoclave

5.1: sodium hydroxide; water / tetrahydrofuran / 40 °C

6.1: thionyl chloride / N,N-dimethyl-formamide / 2 h / Reflux

7.1: dichloromethane; diethyl ether / 1 h / -10 - 0 °C

7.2: 1 h / -10 °C

With thionyl chloride; water; hydrogen bromide; bromine; sodium carbonate; triethylamine; sodium hydroxide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N,N-dimethyl-formamide; In tetrahydrofuran; diethyl ether; dichloromethane; water; toluene; 3.1: Suzuki Coupling;

Reference yield:

: 15155-41-6
4,7-dibromobenzo[c][1,2,5]thiadiazole

: 1312610-44-8
C₁₆H₁₀Br₂N₂O₂S

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water / 12 h / 90 °C / Inert atmosphere

2.1: triethylamine / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 16 h / 120 °C / 15001.5 Torr / Autoclave

3.1: sodium hydroxide; water / tetrahydrofuran / 40 °C

4.1: thionyl chloride / N,N-dimethyl-formamide / 2 h / Reflux

5.1: dichloromethane; diethyl ether / 1 h / -10 - 0 °C

5.2: 1 h / -10 °C

With thionyl chloride; water; sodium carbonate; triethylamine; sodium hydroxide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N,N-dimethyl-formamide; In tetrahydrofuran; diethyl ether; dichloromethane; water; toluene; 1.1: Suzuki Coupling;