mesityl[2-(methoxycarbonyl)phenyl]iodonium trifluoromethanesulfonate

Base Information

• Chemical Name: mesityl[2-(methoxycarbonyl)phenyl]iodonium trifluoromethanesulfonate
• CAS No.: 1203709-71-0
• Molecular Formula: CF₃O₃S*C₁₇H₁₈IO₂
• Molecular Weight: 530.304

Synonyms:mesityl[2-(methoxycarbonyl)phenyl]iodonium trifluoromethanesulfonate

Chemical Property of mesityl[2-(methoxycarbonyl)phenyl]iodonium trifluoromethanesulfonate

Chemical Property:

Purity/Quality:

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Technology Process of mesityl[2-(methoxycarbonyl)phenyl]iodonium trifluoromethanesulfonate

There total 2 articles about mesityl[2-(methoxycarbonyl)phenyl]iodonium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

trifluorormethanesulfonic acid (1493-13-6) + o-iodo-methyl-benzoic acid (610-97-9) + 1,3,5-trimethyl-benzene (108-67-8) → mesityl[2-(methoxycarbonyl)phenyl]iodonium trifluoromethanesulfonate (1203709-71-0)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 40 ℃; for 3.16667h;

DOI:10.1002/anie.201605999

Reference yield:

o-iodo-methyl-benzoic acid (610-97-9) + 1,3,5-trimethyl-benzene (108-67-8) → mesityl[2-(methoxycarbonyl)phenyl]iodonium trifluoromethanesulfonate (1203709-71-0)

Guidance literature:

With trifluorormethanesulfonic acid; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1016/j.jfluchem.2015.09.015

Reference yield: 90.0%

3-phenyl-[1,2,4]triazolo[4,3-a]pyridine (778-65-4) + mesityl[2-(methoxycarbonyl)phenyl]iodonium trifluoromethanesulfonate (1203709-71-0) → 2-(2-(methoxycarbonyl)phenyl)-3-phenyl-[1,2,4]triazolo[4,3-a]pyridin-2-ium trifluoromethanesulfonate

Guidance literature:

With copper(II) bis(trifluoromethanesulfonate); In 1,2-dichloro-ethane; at 110 ℃; for 3h;

DOI:10.1039/C8OB01818A

upstream raw materials:

trifluorormethanesulfonic acid

o-iodo-methyl-benzoic acid

1,3,5-trimethyl-benzene

Downstream raw materials:

2-trifluoromethyl-benzoic acid methyl ester

methyl 2-[1H-indol-2-yl]benzoate

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