Technology Process of C53H84N4O15*C2HF3O2
There total 7 articles about C53H84N4O15*C2HF3O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 12 h / 20 °C
2: triethylamine hydrofluoride / tetrahydrofuran / 12 h / 20 °C
3: dmap; dicyclohexyl-carbodiimide / dichloromethane / 2 h / 20 °C
4: dichloromethane / 1 h / 20 °C
With
dmap; triethylamine hydrofluoride; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; dichloromethane;
DOI:10.1016/j.ejmech.2012.06.044
- Guidance literature:
-
Multi-step reaction with 6 steps
1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 2 h / 20 °C
2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 12 h / 20 °C / 760.05 Torr
3: dmap; dicyclohexyl-carbodiimide / dichloromethane / 12 h / 20 °C
4: triethylamine hydrofluoride / tetrahydrofuran / 12 h / 20 °C
5: dmap; dicyclohexyl-carbodiimide / dichloromethane / 2 h / 20 °C
6: dichloromethane / 1 h / 20 °C
With
dmap; palladium 10% on activated carbon; hydrogen; triethylamine hydrofluoride; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; dichloromethane; ethyl acetate;
DOI:10.1016/j.ejmech.2012.06.044