2,2--1-(2,4,6-tri-tert-butylphenyl)stannaphosphene

Base Information

Chemical Name:2,2--1-(2,4,6-tri-tert-butylphenyl)stannaphosphene
CAS No.:99532-17-9
Molecular Formula:C₃₂H₆₇PSi₄Sn
Molecular Weight:713.91
Hs Code.:

2,2-<bis(trimethylsilyl)methyl>-1-(2,4,6-tri-tert-butylphenyl)stannaphosphene

Synonyms:2,2--1-(2,4,6-tri-tert-butylphenyl)stannaphosphene

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Chemical Property of 2,2--1-(2,4,6-tri-tert-butylphenyl)stannaphosphene

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Technology Process of 2,2--1-(2,4,6-tri-tert-butylphenyl)stannaphosphene

There total 1 articles about 2,2--1-(2,4,6-tri-tert-butylphenyl)stannaphosphene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99532-18-0
(((CH₃)3Si)2CH)2Sn(F)P(H)C₆H₂(C(CH₃)3)3

: 83115-14-4
meso-bis(2,4,6-tri-tert-butylphenyl)diphosphene

: 41823-72-7
bis[bis(trimethylsilyl)methyl]tin(II)

: (((CH₃)3Si)2CH)2Sn(H)P(H)C₆H₂(C(CH₃)3)3

: 99532-17-9
2,2--1-(2,4,6-tri-tert-butylphenyl)stannaphosphene

Guidance literature:: With tert.-butyl lithium; In tetrahydrofuran; at -50 - 25 ℃;
DOI:10.1021/ja00312a088

Reference yield: 77.0%

: 99532-17-9
2,2--1-(2,4,6-tri-tert-butylphenyl)stannaphosphene

: 79073-99-7
bis(2,4,6-tri-tert-butylphenyl)diphosphene

: (CH(Si(CH₃)3)2)2Sn(CH(Si(CH₃)3)2)2

Guidance literature:: In tetrahydrofuran; heating of soln. of starting compound in thf in a sealed tube at 70°C for 15 h; chromy.;

Reference yield: 68.0%

: 7782-49-2
selenium

: 99532-17-9
2,2--1-(2,4,6-tri-tert-butylphenyl)stannaphosphene

: 79073-99-7
bis(2,4,6-tri-tert-butylphenyl)diphosphene

: 117834-22-7
(CH(Si(CH₃)3)2)2Sn(SeSe)PC₆H₂(C(CH₃)3)3

: 117834-21-6
(CH(Si(CH₃)3)2)2Sn(SeSe)Sn(CH(Si(CH₃)3)2)2

Guidance literature:: In tetrahydrofuran; pentane; Se is added to a soln. of the tin-compd. under N2 at 0°C, warming to room temp.; after 1 h intermediate dissappears (monitored by NMR-spectroscopy), removal of solvent under vac., addn. of pentane, crystn., elem. anal., chromy.;