2,4-di-O-benzoyl-3,6-di-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranosyl amine

Base Information

• Chemical Name: 2,4-di-O-benzoyl-3,6-di-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranosyl amine
• CAS No.: 639464-26-9
• Molecular Formula: C₄₈H₅₇NO₂₅
• Molecular Weight: 1047.97

Synonyms:2,4-di-O-benzoyl-3,6-di-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranosyl amine

Chemical Property of 2,4-di-O-benzoyl-3,6-di-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranosyl amine

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Technology Process of 2,4-di-O-benzoyl-3,6-di-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranosyl amine

There total 2 articles about 2,4-di-O-benzoyl-3,6-di-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranosyl amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

2,4-di-O-benzoyl-3,6-di-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranosyl azide → 2,4-di-O-benzoyl-3,6-di-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranosyl amine (639464-26-9)

Guidance literature:

With hydrogen; ammonium formate; palladium on activated charcoal; In methanol; at 70 ℃; for 1h;

DOI:10.1002/anie.200601123

Reference yield: 37.0%

2,4-di-O-benzoyl-3,6-di-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranosyl azide → 2,4-di-O-benzoyl-3,6-di-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranosyl amine (639464-26-9)

Guidance literature:

With 1.3-propanedithiol; N-ethyl-N,N-diisopropylamine; In methanol; at 20 ℃; for 4.5h;

DOI:10.1039/b301670f

Reference yield: 86.0%

(S)-2-[{({9H-fluoren-9-yl}methoxy)carbonyl}amino]pentanedioic acid (104091-09-0,136083-74-4,121343-82-6) + 2,4-di-O-benzoyl-3,6-di-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranosyl amine (639464-26-9) → C116H129N3O54

Guidance literature:

With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; diisopropyl-carbodiimide; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

DOI:10.1002/anie.200601123

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