S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-[(N-hydroxy-N-methyl)-carbamoyl]sulfoximide

Base Information

Chemical Name:S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-[(N-hydroxy-N-methyl)-carbamoyl]sulfoximide
CAS No.:1147096-11-4
Molecular Formula:C₂₂H₁₉Cl₂N₅O₅S
Molecular Weight:536.395
Hs Code.:

Synonyms:S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-[(N-hydroxy-N-methyl)-carbamoyl]sulfoximide

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Chemical Property of S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-[(N-hydroxy-N-methyl)-carbamoyl]sulfoximide

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Technology Process of S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-[(N-hydroxy-N-methyl)-carbamoyl]sulfoximide

There total 11 articles about S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-[(N-hydroxy-N-methyl)-carbamoyl]sulfoximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1147096-10-3
S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-[(N-methoxy-N-methyl)-carbamoyl]sulfoximide

: 1147096-11-4
S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-[(N-hydroxy-N-methyl)-carbamoyl]sulfoximide

Guidance literature:: S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-[(N-methoxy-N-methyl)-carbamoyl]sulfoximide; With boron tribromide; In dichloromethane; at -50 - 30 ℃; for 2h; Inert atmosphere;

With water; Cooling;

Reference yield:

: 3795-79-7
methyl 4-(methylthio)benzoate

: 1147096-11-4
S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-[(N-hydroxy-N-methyl)-carbamoyl]sulfoximide

Guidance literature:: Multi-step reaction with 9 steps

1.1: vanadia / acetonitrile / -25 - -20 °C / Inert atmosphere

1.2: 25 - 30 °C

2.1: sodium azide; sulfuric acid / chloroform / 15 h / -20 - 50 °C / Inert atmosphere

3.1: pyridine / dichloromethane / 3 h / 15 - 30 °C / Inert atmosphere

4.1: sodium hydroxide; water / tetrahydrofuran / 3 h / 25 - 30 °C

4.2: 0 °C

5.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 3 h / 10 - 30 °C / Inert atmosphere

6.1: tetrahydrofuran / 12 h / 10 - 30 °C / Inert atmosphere

7.1: sulfuric acid / 0 - 5 °C

8.1: pyridine / 15 h / 0 - 30 °C / Inert atmosphere

9.1: boron tribromide / dichloromethane / 2 h / -50 - 30 °C / Inert atmosphere

9.2: Cooling

With pyridine; sodium azide; oxalyl dichloride; sulfuric acid; water; vanadia; boron tribromide; sodium hydroxide; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; chloroform; acetonitrile;

Reference yield:

: 1147096-52-3
methyl 4-(N-((benzyloxy)carbonyl)-S-methylsulfonimidoyl)benzoate

: 1147096-11-4
S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-[(N-hydroxy-N-methyl)-carbamoyl]sulfoximide

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydroxide; water / tetrahydrofuran / 3 h / 25 - 30 °C

1.2: 0 °C

2.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 3 h / 10 - 30 °C / Inert atmosphere

3.1: tetrahydrofuran / 12 h / 10 - 30 °C / Inert atmosphere

4.1: sulfuric acid / 0 - 5 °C

5.1: pyridine / 15 h / 0 - 30 °C / Inert atmosphere

6.1: boron tribromide / dichloromethane / 2 h / -50 - 30 °C / Inert atmosphere

6.2: Cooling

With pyridine; oxalyl dichloride; sulfuric acid; water; boron tribromide; sodium hydroxide; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane;