dibenzyl (2-acetonyl-2-deoxy-3,4,6-tri-O-acetyl-α-D-glucopyranosyl) phosphate

Base Information

Chemical Name:dibenzyl (2-acetonyl-2-deoxy-3,4,6-tri-O-acetyl-α-D-glucopyranosyl) phosphate
CAS No.:1286737-87-8
Molecular Formula:C₂₉H₃₅O₁₂P
Molecular Weight:606.563
Hs Code.:

Synonyms:dibenzyl (2-acetonyl-2-deoxy-3,4,6-tri-O-acetyl-α-D-glucopyranosyl) phosphate

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Chemical Property of dibenzyl (2-acetonyl-2-deoxy-3,4,6-tri-O-acetyl-α-D-glucopyranosyl) phosphate

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Technology Process of dibenzyl (2-acetonyl-2-deoxy-3,4,6-tri-O-acetyl-α-D-glucopyranosyl) phosphate

There total 3 articles about dibenzyl (2-acetonyl-2-deoxy-3,4,6-tri-O-acetyl-α-D-glucopyranosyl) phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₀H₃₇O₁₀P

: 1286737-87-8
dibenzyl (2-acetonyl-2-deoxy-3,4,6-tri-O-acetyl-α-D-glucopyranosyl) phosphate

Guidance literature:: C₃₀H₃₇O₁₀P; With ozone; In dichloromethane; at -78 ℃;

With dimethylsulfide; In dichloromethane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2011.01.081

Reference yield:

: 108549-23-1
Dibenzyl N,N-diisopropylphosphoramidite

: 1286737-87-8
dibenzyl (2-acetonyl-2-deoxy-3,4,6-tri-O-acetyl-α-D-glucopyranosyl) phosphate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1H-tetrazole / dichloromethane / 3 h / -30 - 20 °C / Inert atmosphere

2.1: ozone / dichloromethane / -78 °C

2.2: -78 - 20 °C / Inert atmosphere

With 1H-tetrazole; ozone; In dichloromethane;
DOI:10.1016/j.tet.2011.01.081

Reference yield:

: 3,4,6-tri-O-acetyl-2-deoxy-2-(methallyl)-D-glucopyranose

: 1286737-87-8
dibenzyl (2-acetonyl-2-deoxy-3,4,6-tri-O-acetyl-α-D-glucopyranosyl) phosphate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1H-tetrazole / dichloromethane / 3 h / -30 - 20 °C / Inert atmosphere

2.1: ozone / dichloromethane / -78 °C

2.2: -78 - 20 °C / Inert atmosphere

With 1H-tetrazole; ozone; In dichloromethane;
DOI:10.1016/j.tet.2011.01.081