17,17'-(1,3-phenylene)ditritriacontan-17-ol

Base Information

• Chemical Name: 17,17'-(1,3-phenylene)ditritriacontan-17-ol
• CAS No.: 1350559-68-0
• Molecular Formula: C₇₂H₁₃₈O₂
• Molecular Weight: 1035.89
• Mol file: 1350559-68-0.mol

Synonyms:17,17'-(1,3-phenylene)ditritriacontan-17-ol

Chemical Property of 17,17'-(1,3-phenylene)ditritriacontan-17-ol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 17,17'-(1,3-phenylene)ditritriacontan-17-ol

There total 1 articles about 17,17'-(1,3-phenylene)ditritriacontan-17-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

dimethyl Isophthalate (1459-93-4) → 17,17'-(1,3-phenylene)ditritriacontan-17-ol (1350559-68-0)

Guidance literature:

In diethyl ether; at 20 ℃; for 12h;

DOI:10.1002/adsc.201100278

Reference yield:

17,17'-(1,3-phenylene)ditritriacontan-17-ol (1350559-68-0) → 1,3-di(tritriacontan-17-yl)benzene (1350559-70-4)

Guidance literature:

17,17'-(1,3-phenylene)ditritriacontan-17-ol; With toluene-4-sulfonic acid; In toluene; Reflux;

With 5%-palladium/activated carbon; hydrogen; In tetrahydrofuran; at 40 ℃; for 12h; under 3000.3 Torr;

DOI:10.1002/adsc.201100278

Reference yield:

17,17'-(1,3-phenylene)ditritriacontan-17-ol (1350559-68-0) → 2,4-di(tritriacontan-17-yl)benzenesulfonic acid (1350559-71-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: toluene-4-sulfonic acid / toluene / Reflux

1.2: 12 h / 40 °C / 3000.3 Torr

2.1: sulfuric acid / dichloromethane / 0.08 h

With sulfuric acid; toluene-4-sulfonic acid; In dichloromethane; toluene;

DOI:10.1002/adsc.201100278

upstream raw materials:

dimethyl Isophthalate

Downstream raw materials:

1,3-di(tritriacontan-17-yl)benzene

2,4-di(tritriacontan-17-yl)benzenesulfonic acid

Refernces